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Synthesis of a water-soluble 1,3-bis(diphenylene)-2-phenylallyl radical.


ABSTRACT: The design and synthesis of a water-soluble 1,3-bis(diphenylene)-2-phenylallyl (BDPA) radical via the conjugate addition of a derivatized fluorene nucelophile is described. The compound is designed for use in dynamic nuclear polarization NMR. Its 9 GHz EPR spectrum in glycerol/water is reported.

SUBMITTER: Dane EL 

PROVIDER: S-EPMC2882179 | biostudies-literature | 2010 May

REPOSITORIES: biostudies-literature

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Synthesis of a water-soluble 1,3-bis(diphenylene)-2-phenylallyl radical.

Dane Eric L EL   Swager Timothy M TM  

The Journal of organic chemistry 20100501 10


The design and synthesis of a water-soluble 1,3-bis(diphenylene)-2-phenylallyl (BDPA) radical via the conjugate addition of a derivatized fluorene nucelophile is described. The compound is designed for use in dynamic nuclear polarization NMR. Its 9 GHz EPR spectrum in glycerol/water is reported. ...[more]

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