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3,4-Dihydr-oxy-N'-(2-hydroxy-benzyl-idene)benzohydrazide-methanol-water (2/1/3).

ABSTRACT: The asymmetric unit of the title compound, C(14)H(12)N(2)O(4)·0.5CH(4)O·1.5H(2)O, consists of two Schiff base mol-ecules, three water mol-ecules and one methanol mol-ecule. The dihedral angle between the two benzene rings is 7.8?(2)° in one of the mol-ecules and 4.0?(2)° in the other. Intra-molecular O-H?O and O-H?N hydrogen bonds are observed. Mol-ecules are linked into a three-dimensional network by O-H?O and N-H?O inter-molecular hydrogen bonds.

SUBMITTER: Ma HB

PROVIDER: S-EPMC2915271 | biostudies-literature | 2007 Dec

REPOSITORIES: biostudies-literature

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3,4-Dihydr-oxy-N'-(2-hydroxy-benzyl-idene)benzohydrazide-methanol-water (2/1/3).

Ma Hong-Bo HB Huang Shan-Shan SS Diao Yun-Peng YP

Acta crystallographica. Section E, Structure reports online 20071206 Pt 1

The asymmetric unit of the title compound, C(14)H(12)N(2)O(4)·0.5CH(4)O·1.5H(2)O, consists of two Schiff base mol-ecules, three water mol-ecules and one methanol mol-ecule. The dihedral angle between the two benzene rings is 7.8 (2)° in one of the mol-ecules and 4.0 (2)° in the other. Intra-molecular O-H⋯O and O-H⋯N hydrogen bonds are observed. Mol-ecules are linked into a three-dimensional network by O-H⋯O and N-H⋯O inter-molecular hydrogen bonds. ...[more]

PMID: 21200776

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