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6,6'-Dibromo-2,2'-dihex-yloxy-1,1'-bi-naphthalene.


ABSTRACT: The title compound, C(32)H(36)Br(2)O(2), was prepared by the reaction of 6-bromo-1-(2-bromo-6-hydroxy-naphthalen-5-yl)-naphthalen-2-ol and 1-iodo-hexane. The dihedral angle between the naphthalene ring planes is 63.8?(9)° The crystal structure may be stabilized by two very weak ?-? inter-actions involving the six-membered rings, with centroid-centroid distances of 4.012?(4) and 4.010?(4)?Å. The crystal studied was an inversion twin.

SUBMITTER: Li YF 

PROVIDER: S-EPMC2959541 | biostudies-literature | 2008 Oct

REPOSITORIES: biostudies-literature

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6,6'-Dibromo-2,2'-dihex-yloxy-1,1'-bi-naphthalene.

Li Yu-Feng YF   Wang Lin-Tong LT   Jian Fang-Fang FF  

Acta crystallographica. Section E, Structure reports online 20081018 Pt 11


The title compound, C(32)H(36)Br(2)O(2), was prepared by the reaction of 6-bromo-1-(2-bromo-6-hydroxy-naphthalen-5-yl)-naphthalen-2-ol and 1-iodo-hexane. The dihedral angle between the naphthalene ring planes is 63.8 (9)° The crystal structure may be stabilized by two very weak π-π inter-actions involving the six-membered rings, with centroid-centroid distances of 4.012 (4) and 4.010 (4) Å. The crystal studied was an inversion twin. ...[more]

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