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2-(1H-1,2,3-Benzotriazol-1-yl)-N'-cyclo-pentyl-ideneacetohydrazide.

ABSTRACT: The title compound, C(13)H(15)N(5)O, was synthesized by the reaction of 2-(1H-1,2,3-benzotriazol-1-yl)acetohydrazide with cyclo-penta-none. In the cyclopentane ring, two C atoms and their attached H atoms are disordered over two positions; the site occupancy factors are ca 0.63 and 0.37. In the crystal structure, mol-ecules are linked into infinite chains directed along the b axis by N-H?O hydrogen bonds. In addition, there are weak C-H?O and C-H?N hydrogen bonds, as well as C-H??-ring inter-actions in the structure.

SUBMITTER: Ji NN

PROVIDER: S-EPMC2961015 | biostudies-literature | 2008 Mar

REPOSITORIES: biostudies-literature

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2-(1H-1,2,3-Benzotriazol-1-yl)-N'-cyclo-pentyl-ideneacetohydrazide.

Ji Ning-Ning NN Shi Zhi-Qiang ZQ

Acta crystallographica. Section E, Structure reports online 20080305 Pt 4

The title compound, C(13)H(15)N(5)O, was synthesized by the reaction of 2-(1H-1,2,3-benzotriazol-1-yl)acetohydrazide with cyclo-penta-none. In the cyclopentane ring, two C atoms and their attached H atoms are disordered over two positions; the site occupancy factors are ca 0.63 and 0.37. In the crystal structure, mol-ecules are linked into infinite chains directed along the b axis by N-H⋯O hydrogen bonds. In addition, there are weak C-H⋯O and C-H⋯N hydrogen bonds, as well as C-H⋯π-ring inter-act ...[more]

PMID: 21202052

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