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N-(2-Chloro-4-nitro-phen-yl)-2-nitro-benzamide.

ABSTRACT: In the title compound, C(13)H(8)ClN(3)O(5), the dihedral angle between the two aromatic rings is 70.74?(6)°. The nitro groups of the Cl-substituted and benzamide benzene rings are twisted by 2.6?(1) and 31.3?(2)°, respectively. The crystal packing shows inter-molecular C-H?O hydrogen bonds that link mol-ecules into sheets stacked along [010].

SUBMITTER: Saeed A

PROVIDER: S-EPMC2961029 | biostudies-literature | 2008 Mar

REPOSITORIES: biostudies-literature

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N-(2-Chloro-4-nitro-phen-yl)-2-nitro-benzamide.

Saeed Aamer A Hussain Shahid S Flörke Ulrich U

Acta crystallographica. Section E, Structure reports online 20080312 Pt 4

In the title compound, C(13)H(8)ClN(3)O(5), the dihedral angle between the two aromatic rings is 70.74 (6)°. The nitro groups of the Cl-substituted and benzamide benzene rings are twisted by 2.6 (1) and 31.3 (2)°, respectively. The crystal packing shows inter-molecular C-H⋯O hydrogen bonds that link mol-ecules into sheets stacked along [010]. ...[more]

PMID: 21202096

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N-(4-Chloro-phen-yl)-4-nitro-benzamide.

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Crystal structure of 3-chloro-N-(2-nitro-phen-yl)benzamide.

Project description:In the title compound, C13H9ClN2O3, the mean plane of the central amide fragment (r.m.s. deviation = 0.016 Å) subtends dihedral angles of 15.2 (2) and 8.2 (2)° with the chloro- and nitro-substituted benzene rings, respectively. An intra-molecular N-H⋯O hydrogen bond generates an S(6) ring. In the crystal, mol-ecules are linked by weak C-H⋯O hydrogen bonds, forming C(7) chains which propagate along [010], but no Cl⋯Cl short contacts are observed.

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N-(2-Nitro-phen-yl)benzamide.

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3-Chloro-N-(2-chloro-phen-yl)benzamide.

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