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(E)-1-(3-Methoxy-phen-yl)ethanone 4-nitro-phenyl-hydrazone.

ABSTRACT: Crystals of the title compound, C(15)H(15)N(3)O(3), were obtained from a condensation reaction of 4-nitro-phenyl-hydrazine and 3-methoxy-acetophenone. In the crystal structure, the methoxy-phenyl ring is twisted slightly with respect to the nitro-phenyl-hydrazine plane, making a dihedral angle of 14.81?(8)°. The nitro and meth-oxy groups are each coplanar with the attached benzene rings. The nitro-phenyl and methoxy-phenyl groups are located on opposite sides of the C=N double bond, indicating an E configuration of the mol-ecule. Adjacent mol-ecules are linked together via N-H?O hydrogen bonding, forming chains along the [101] direction.

SUBMITTER: Fan Z

PROVIDER: S-EPMC2961743 | biostudies-literature | 2008 Jun

REPOSITORIES: biostudies-literature

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(E)-1-(3-Methoxy-phen-yl)ethanone 4-nitro-phenyl-hydrazone.

Fan Zheng Z Shan Shang S Wang Shan-Heng SH Wang Wen-Long WL

Acta crystallographica. Section E, Structure reports online 20080625 Pt 7

Crystals of the title compound, C(15)H(15)N(3)O(3), were obtained from a condensation reaction of 4-nitro-phenyl-hydrazine and 3-methoxy-acetophenone. In the crystal structure, the methoxy-phenyl ring is twisted slightly with respect to the nitro-phenyl-hydrazine plane, making a dihedral angle of 14.81 (8)°. The nitro and meth-oxy groups are each coplanar with the attached benzene rings. The nitro-phenyl and methoxy-phenyl groups are located on opposite sides of the C=N double bond, indicating a ...[more]

PMID: 21202963

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