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Aqua-(propane-dioato-?O,O)[2-(1H-pyrazol-1-yl-?N)-1,10-phenanthroline-?N,N']nickel(II) trihydrate.

ABSTRACT: In the title mononuclear complex, [Ni(C(3)H(2)O(4))(C(15)H(10)N(4))(H(2)O)]·3H(2)O, the metal center is coordinated in a distorted NiN(3)O(3) geometry. In the crystal structure, inter-molecular O-H?O hydrogen bonds link the components into a two-dimensional network. In addition, there are weak ?-? stacking inter-actions between symmetry-related phenanthroline rings, with a centroid-centroid distance of 3.6253?(17)?Å.

SUBMITTER: Yan HY 

PROVIDER: S-EPMC2969757 | biostudies-literature | 2009 May

REPOSITORIES: biostudies-literature

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Aqua-(propane-dioato-κO,O)[2-(1H-pyrazol-1-yl-κN)-1,10-phenanthroline-κN,N']nickel(II) trihydrate.

Yan Huai Yi HY   Hu Tai Qiu TQ   Shi Jing Min JM  

Acta crystallographica. Section E, Structure reports online 20090514 Pt 6

In the title mononuclear complex, [Ni(C(3)H(2)O(4))(C(15)H(10)N(4))(H(2)O)]·3H(2)O, the metal center is coordinated in a distorted NiN(3)O(3) geometry. In the crystal structure, inter-molecular O-H⋯O hydrogen bonds link the components into a two-dimensional network. In addition, there are weak π-π stacking inter-actions between symmetry-related phenanthroline rings, with a centroid-centroid distance of 3.6253 (17) Å. ...[more]

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