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1-(4-Bromo-phen-yl)-3-(2-thienylcarbon-yl)thio-urea.

ABSTRACT: The title compound, C(12)H(9)BrN(2)OS(2), consists of two planar parts, viz. the thio-phene ring including all substituents (r.m.s. deviation 0.007?Å) and the benzene ring including the respective substituents as well as the thione group (r.m.s. deviation 0.05?Å). The inter-planar angle is 18.84?(6)°. An intra-molecular C(phen-yl)-N-H?OC hydrogen bond is observed. The three-dimensional packing involves three types of inter-actions, viz. N-H?S, C-H?S (× 2) and Br?S [3.6924?(6)?Å].

SUBMITTER: Saeed S

PROVIDER: S-EPMC2970465 | biostudies-literature | 2009 Sep

REPOSITORIES: biostudies-literature

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1-(4-Bromo-phen-yl)-3-(2-thienylcarbon-yl)thio-urea.

Saeed Sohail S Rashid Naghmana N Hussain Rizwan R Jones Peter G PG

Acta crystallographica. Section E, Structure reports online 20090930 Pt 10

The title compound, C(12)H(9)BrN(2)OS(2), consists of two planar parts, viz. the thio-phene ring including all substituents (r.m.s. deviation 0.007 Å) and the benzene ring including the respective substituents as well as the thione group (r.m.s. deviation 0.05 Å). The inter-planar angle is 18.84 (6)°. An intra-molecular C(phen-yl)-N-H⋯OC hydrogen bond is observed. The three-dimensional packing involves three types of inter-actions, viz. N-H⋯S, C-H⋯S (× 2) and Br⋯S [3.6924 (6) Å]. ...[more]

PMID: 21578006

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