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5-(4-Phenoxy-phen-yl)-1,3,4-thia-diazol-2-amine.

ABSTRACT: The title compound, C(14)H(11)N(3)OS, was synthesized by the reaction of phenoxy-benzoic acid and thio-semicarbazide. The thia-diazole ring makes dihedral angles of 0.99?(16) and 86.53?(18)°, respectively, with the benzene and phenyl rings. The dihedral angle between the benzene and phenyl rings is 87.17?(19)°. Intra-molecular C-H?S contacts are present. In the crystal, inter-molecular N-H?N hydrogen bonds link the mol-ecules.

SUBMITTER: Wan R

PROVIDER: S-EPMC2977727 | biostudies-literature | 2009 Apr

REPOSITORIES: biostudies-literature

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5-(4-Phenoxy-phen-yl)-1,3,4-thia-diazol-2-amine.

Wan Rong R Wang Yao Y Han Feng F Wang Peng P

Acta crystallographica. Section E, Structure reports online 20090418 Pt 5

The title compound, C(14)H(11)N(3)OS, was synthesized by the reaction of phenoxy-benzoic acid and thio-semicarbazide. The thia-diazole ring makes dihedral angles of 0.99 (16) and 86.53 (18)°, respectively, with the benzene and phenyl rings. The dihedral angle between the benzene and phenyl rings is 87.17 (19)°. Intra-molecular C-H⋯S contacts are present. In the crystal, inter-molecular N-H⋯N hydrogen bonds link the mol-ecules. ...[more]

PMID: 21583863

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