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2-Iodo-5-nitro-thio-phene.

ABSTRACT: The title compound, C(4)H(2)INO(2)S, was synthesized by nitration of iodo-thio-phene with acetyl nitrate. The molecule is essentially planar, withthe nitro group tilted by 1.78?(19)° and the iodine atom displaced by 0.0233?(2)?Å with respect to the thiophene ring. In the crystal structure, adjacent mol-ecules are linked through weak I?O inter-actions [3.039?(2)Å], forming chains extending along the b axis.

SUBMITTER: Xu XY

PROVIDER: S-EPMC2979622 | biostudies-literature | 2010 May

REPOSITORIES: biostudies-literature

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2-Iodo-5-nitro-thio-phene.

Xu Xing Yan XY Huang Gang G Zeng Xiang Chao XC Hu Fang F

Acta crystallographica. Section E, Structure reports online 20100522 Pt 6

The title compound, C(4)H(2)INO(2)S, was synthesized by nitration of iodo-thio-phene with acetyl nitrate. The molecule is essentially planar, withthe nitro group tilted by 1.78 (19)° and the iodine atom displaced by 0.0233 (2) Å with respect to the thiophene ring. In the crystal structure, adjacent mol-ecules are linked through weak I⋯O inter-actions [3.039 (2)Å], forming chains extending along the b axis. ...[more]

PMID: 21579486

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