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12-Eth-oxy-2,3,8,9-tetra-methoxy-benzo[c]phenanthridine dichloro-methane solvate.

ABSTRACT: The title compound, C(23)H(23)NO(5)·CH(2)Cl(2), was obtained via the alkyl-ation of the 12-hydr-oxy-2,3,8,9-tetra-methoxy-benzo[c]phenanthridine salt. The benzo[c]phenanthridine ring system is essentially planar, with a mean out-of-plane deviation of 0.026?Å. A dicloromethane mol-ecule of solvation is present and located between the sheets of phenanthridine mol-ecules, preventing any significant inter-molecular hydrogen-bonding or ?-? inter-actions.

SUBMITTER: Ronaldson M

PROVIDER: S-EPMC2980059 | biostudies-literature | 2009 Dec

REPOSITORIES: biostudies-literature

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12-Eth-oxy-2,3,8,9-tetra-methoxy-benzo[c]phenanthridine dichloro-methane solvate.

Ronaldson Michael M Maheux Chad R CR Nyangulu James M JM Cameron T Stanley TS Aquino Manuel A S MA

Acta crystallographica. Section E, Structure reports online 20091212 Pt 1

The title compound, C(23)H(23)NO(5)·CH(2)Cl(2), was obtained via the alkyl-ation of the 12-hydr-oxy-2,3,8,9-tetra-methoxy-benzo[c]phenanthridine salt. The benzo[c]phenanthridine ring system is essentially planar, with a mean out-of-plane deviation of 0.026 Å. A dicloromethane mol-ecule of solvation is present and located between the sheets of phenanthridine mol-ecules, preventing any significant inter-molecular hydrogen-bonding or π-π inter-actions. ...[more]

PMID: 21580014

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