Unknown

Dataset Information

0

12-Eth-oxy-2,3,8,9-tetra-methoxy-benzo[c]phenanthridine dichloro-methane solvate.

ABSTRACT: The title compound, C(23)H(23)NO(5)·CH(2)Cl(2), was obtained via the alkyl-ation of the 12-hydr-oxy-2,3,8,9-tetra-methoxy-benzo[c]phenanthridine salt. The benzo[c]phenanthridine ring system is essentially planar, with a mean out-of-plane deviation of 0.026?Å. A dicloromethane mol-ecule of solvation is present and located between the sheets of phenanthridine mol-ecules, preventing any significant inter-molecular hydrogen-bonding or ?-? inter-actions.

SUBMITTER: Ronaldson M 

PROVIDER: S-EPMC2980059 | biostudies-literature | 2009 Dec

REPOSITORIES: biostudies-literature

Json Xml
altmetric image

Publications

12-Eth-oxy-2,3,8,9-tetra-methoxy-benzo[c]phenanthridine dichloro-methane solvate.

Ronaldson Michael M   Maheux Chad R CR   Nyangulu James M JM   Cameron T Stanley TS   Aquino Manuel A S MA  

Acta crystallographica. Section E, Structure reports online 20091212 Pt 1

The title compound, C(23)H(23)NO(5)·CH(2)Cl(2), was obtained via the alkyl-ation of the 12-hydr-oxy-2,3,8,9-tetra-methoxy-benzo[c]phenanthridine salt. The benzo[c]phenanthridine ring system is essentially planar, with a mean out-of-plane deviation of 0.026 Å. A dicloromethane mol-ecule of solvation is present and located between the sheets of phenanthridine mol-ecules, preventing any significant inter-molecular hydrogen-bonding or π-π inter-actions. ...[more]

Similar Datasets

Unknown 1,3-Dimesitylimidazolidinium tetra-chloridogold(III) dichloro-methane solvate.
| S-EPMC2959617 | biostudies-literature
Unknown 4-Des-oxy-4?-(4-methoxy-carbonyl-1,2,3-triazol-1-yl)podophyllotoxin dichloro-methane solvate.
| S-EPMC2971900 | biostudies-other
Unknown [5,10,15,20-Tetra-kis(4-tol-yl)porphyrin]zinc(II) dichloro-methane solvate.
| S-EPMC3006952 | biostudies-literature
Unknown 5,11,17,23-Tetra-tert-butyl-25,27-bis-[2-(4-nitro-phen-oxy)eth-oxy]calix[4]arene-26,28-diol acetonitrile tetra-solvate.
| S-EPMC2969685 | biostudies-literature
Unknown 5,11,17,23-Tetra-tert-butyl-25,26,27,28-tetra-methoxy-calix[4]arene dichloro-methane hemisolvate.
| S-EPMC2960888 | biostudies-other
Unknown N-[3,5-Dichloro-4-(1,1,2,2-tetra-fluoro-eth-oxy)phen-yl]-2,6-difluoro-benzamide.
| S-EPMC3007377 | biostudies-literature
Unknown 1-(2,6-Dichloro-benzo-yl)-3-(2,3,5,6-tetra-chloro-phen-yl)thio-urea trichloro-methane hemisolvate.
| S-EPMC2968195 | biostudies-literature
Unknown 5-(4-Bromo-phen-yl)-1,2,3,4-tetra-hydro-benzo[a]phenanthridine.
| S-EPMC2977753 | biostudies-literature
Unknown N'-(2,4-Dichloro-benzyl-idene)-4-methoxy-benzohydrazide methanol solvate.
| S-EPMC2969251 | biostudies-literature
Unknown 7-Eth-oxy-4'-methoxy-isoflavone (monoethyl-formononetin).
| S-EPMC2961316 | biostudies-literature