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N,N'-Bis(4-bromo-phen-yl)naphthalene-1,4-dicarboxamide N,N-dimethyl-acetamide disolvate.

ABSTRACT: The title compound, C(24)H(16)Br(2)N(2)O(2)·2C(4)H(9)NO, crystallizes in an anti C=O orientation. The two amide groups are twisted away from the naphthalene ring system by 62.67?(8) and 75.93?(7)°. The crystal packing is stabilized by N-H?O and C-H?O hydrogen bonds. Each of the dimethyl-acetamide solvent mol-ecules is disordered over two positions, with occupancy ratios of 0.556?(7):0.444?(7) and 0.654?(7):0.346?(7).

SUBMITTER: Jing LH

PROVIDER: S-EPMC2980233 | biostudies-literature | 2009 Dec

REPOSITORIES: biostudies-literature

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N,N'-Bis(4-bromo-phen-yl)naphthalene-1,4-dicarboxamide N,N-dimethyl-acetamide disolvate.

Jing Lin-Hai LH

Acta crystallographica. Section E, Structure reports online 20091204 Pt 1

The title compound, C(24)H(16)Br(2)N(2)O(2)·2C(4)H(9)NO, crystallizes in an anti C=O orientation. The two amide groups are twisted away from the naphthalene ring system by 62.67 (8) and 75.93 (7)°. The crystal packing is stabilized by N-H⋯O and C-H⋯O hydrogen bonds. Each of the dimethyl-acetamide solvent mol-ecules is disordered over two positions, with occupancy ratios of 0.556 (7):0.444 (7) and 0.654 (7):0.346 (7). ...[more]

PMID: 21580134

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