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Ethyl 2-[3-(4-nitro-benzo-yl)thio-ureido]benzoate.

ABSTRACT: In the title compound, C(17)H(15)N(3)O(5)S, the nitro and thio-ureido groups are twisted by 7.2?(7) and 21.4?(2)°, respectively, from the nitro-benzene ring plane whereas the thio-ureido and the ethyl ester group make dihedral angles of 43.0?(1) and 18.0?(2)°, respectively, with the benzene rings to which they are attached. Intra-molecular N-H?O hydrogen-bonding inter-actions are observed. In the crystal, inter-molecular N-H?O hydrogen bonds connect the mol-ecules into chains running along the a axis.

SUBMITTER: Saeed S

PROVIDER: S-EPMC2984025 | biostudies-literature | 2010 Mar

REPOSITORIES: biostudies-literature

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Ethyl 2-[3-(4-nitro-benzo-yl)thio-ureido]benzoate.

Saeed Sohail S Rashid Naghmana N Wong Wing-Tak WT

Acta crystallographica. Section E, Structure reports online 20100331 Pt 4

In the title compound, C(17)H(15)N(3)O(5)S, the nitro and thio-ureido groups are twisted by 7.2 (7) and 21.4 (2)°, respectively, from the nitro-benzene ring plane whereas the thio-ureido and the ethyl ester group make dihedral angles of 43.0 (1) and 18.0 (2)°, respectively, with the benzene rings to which they are attached. Intra-molecular N-H⋯O hydrogen-bonding inter-actions are observed. In the crystal, inter-molecular N-H⋯O hydrogen bonds connect the mol-ecules into chains running along the a ...[more]

PMID: 21580777

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