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Methyl 2-[(4-chloro-2-meth-oxy-5-oxo-2,5-dihydro-furan-3-yl)amino]-acetate.

ABSTRACT: The title compound, C(8)H(10)ClNO(5), was obtained via a tandem Michael addition-elimination reaction of 3,4-dichloro-5-meth-oxy-furan-2(5H)-one and glycine methyl ester in the presence of triethyl-amine. The mol-ecular structure contains an approximately planar [maximum atomic deviation = 0.010?(2)?Å] five-membered furan-one ring. The crystal packing is stabilized by inter-molecular N-H?O and weak C-H?O hydrogen bonding.

SUBMITTER: Mo YQ 

PROVIDER: S-EPMC3007059 | biostudies-literature | 2010 Jun

REPOSITORIES: biostudies-literature

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Methyl 2-[(4-chloro-2-meth-oxy-5-oxo-2,5-dihydro-furan-3-yl)amino]-acetate.

Mo Yang-Qing YQ   Wang Zhao-Yang ZY   Fu Jian-Hua JH   Fang Hua-Cai HC  

Acta crystallographica. Section E, Structure reports online 20100630 Pt 7

The title compound, C(8)H(10)ClNO(5), was obtained via a tandem Michael addition-elimination reaction of 3,4-dichloro-5-meth-oxy-furan-2(5H)-one and glycine methyl ester in the presence of triethyl-amine. The mol-ecular structure contains an approximately planar [maximum atomic deviation = 0.010 (2) Å] five-membered furan-one ring. The crystal packing is stabilized by inter-molecular N-H⋯O and weak C-H⋯O hydrogen bonding. ...[more]

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