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N-(6-{2-[6-(2,2-Dimethyl-propanamido)-2-pyrid-yl]eth-yl}-2-pyrid-yl)-2,2-dimethyl-propanamide.

ABSTRACT: The title compound, C(22)H(30)N(4)O(2), lies about a crystallographic inversion center. The whole mol-ecule is disordered over two positions with a refined occupancy ratio of 0.636?(10):0.364?(10). The pyridine rings are approximately planar, with maximum deviations of 0.033?(10) and 0.063?(17)?Å for the major and minor components, respectively. The mean planes of the pyridine rings form dihedral angles of 17?(2)° in the major component and 18?(2)° in the minor component with the respective formamide groups attached to them. In the crystal packing, inter-molecular N-H?O and C-H?O hydrogen bonds link the mol-ecules into two-dimensional networks parallel to the ab plane.

SUBMITTER: Fun HK

PROVIDER: S-EPMC3007361 | biostudies-literature | 2010 Jul

REPOSITORIES: biostudies-literature

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N-(6-{2-[6-(2,2-Dimethyl-propanamido)-2-pyrid-yl]eth-yl}-2-pyrid-yl)-2,2-dimethyl-propanamide.

Fun Hoong-Kun HK Loh Wan-Sin WS Das Nirmal Kumar NK Sen Debabrata D Goswami Shyamaprosad S

Acta crystallographica. Section E, Structure reports online 20100710 Pt 8

The title compound, C(22)H(30)N(4)O(2), lies about a crystallographic inversion center. The whole mol-ecule is disordered over two positions with a refined occupancy ratio of 0.636 (10):0.364 (10). The pyridine rings are approximately planar, with maximum deviations of 0.033 (10) and 0.063 (17) Å for the major and minor components, respectively. The mean planes of the pyridine rings form dihedral angles of 17 (2)° in the major component and 18 (2)° in the minor component with the respective form ...[more]

PMID: 21588283

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