Unknown

Dataset Information

0

1,8-Bis(3-chloro-anilino)-N,N'-bis-(3-chloro-phen-yl)octane-1,8-diimine.

ABSTRACT: There are two half-mol-ecules in the asymmetric unit of the title compound, C(32)H(30)Cl(4)N(4), in both of which the N-H bonds are syn to the meta-chloro substituents in the adjacent benzene ring. The other two Cl atoms of these two mol-ecules are disordered with occunpancy ratios of 0.79 (2):0.21 (2) and 0.68 (1):0.32 (1). Adjacent chloro-phenyl rings make dihedral angles of 74.3 (2) and 63.0 (2)° in the two mol-ecules. In the crystal, inter-molecular N-H⋯N hydrogen bonds link the mol-ecules into infinite chains.

SUBMITTER: Gowda BT 

PROVIDER: S-EPMC3051938 | biostudies-literature | 2011 Feb

REPOSITORIES: biostudies-literature

Json Xml
altmetric image

Publications

1,8-Bis(3-chloro-anilino)-N,N'-bis-(3-chloro-phen-yl)octane-1,8-diimine.

Gowda B Thimme BT   Foro Sabine S   Rodrigues Vinola Z VZ   Spandana H S HS   Fuess Hartmut H  

Acta crystallographica. Section E, Structure reports online 20110212 Pt 3

There are two half-mol-ecules in the asymmetric unit of the title compound, C(32)H(30)Cl(4)N(4), in both of which the N-H bonds are syn to the meta-chloro substituents in the adjacent benzene ring. The other two Cl atoms of these two mol-ecules are disordered with occunpancy ratios of 0.79 (2):0.21 (2) and 0.68 (1):0.32 (1). Adjacent chloro-phenyl rings make dihedral angles of 74.3 (2) and 63.0 (2)° in the two mol-ecules. In the crystal, inter-molecular N-H⋯N hydrogen bonds link the mol-ecules i  ...[more]

Similar Datasets

Unknown 2,2'-Bis(4-fluoro-anilino)-3,3'-(3,6-dioxa-octane-1,8-di-yl)diquinazolin-4(3H)-one.
| S-EPMC2967967 | biostudies-literature
Unknown N,N'-Bis[3,5-bis-(2,6-diisopropyl-phen-yl)phen-yl]butane-2,3-diimine.
| S-EPMC3200583 | biostudies-literature
Unknown 2-(4-Chloro-anilino)-1-(4-chloro-phen-yl)ethanone.
| S-EPMC3239017 | biostudies-literature
Unknown 1,8-Bis(4-fluoro-phen-yl)naphthalene.
| S-EPMC3151928 | biostudies-literature
Unknown Diethyl [(5-chloro-2-hydroxy-anilino)(4-chloro-phen-yl)meth-yl]phospho-nate.
| S-EPMC2970406 | biostudies-literature
Unknown Ethyl 2,6-bis-(4-chloro-phen-yl)-4-(4-fluoro-anilino)-1-(4-fluoro-phen-yl)-1,2,5,6-tetra-hydro-pyridine-3-carboxyl-ate.
| S-EPMC3629536 | biostudies-literature
Unknown Ethyl 2,6-bis-(4-chloro-phen-yl)-4-(4-methyl-anilino)-1-(4-methyl-phen-yl)-1,2,5,6-tetra-hydro-pyridine-3-carboxyl-ate.
| S-EPMC3588410 | biostudies-literature
Unknown (2-Anilino-4-methyl-thia-zol-5-yl)(4-chloro-phen-yl)methanone.
| S-EPMC3254502 | biostudies-literature
Unknown Ethyl 4-anilino-2,6-bis-(4-chloro-phen-yl)-1-phenyl-1,2,5,6-tetra-hydro-pyridine-3-carboxyl-ate.
| S-EPMC3685090 | biostudies-literature
Unknown N,N'-Bis(2,6-diethyl-phen-yl)acenaphthyl-ene-1,2-diimine.
| S-EPMC3254474 | biostudies-literature