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(1-Phenyl-sulfonyl-1H-indol-2-yl)(thio-phen-2-yl)methanone.

ABSTRACT: The crystal studied of the title compound, C(19)H(13)NO(3)S(2), was found to be a non-merohedral twin with a domain ratio of 0.877?(3):0.123?(3). There are two independent mol-ecules in the asymmetric unit. The dihedral angles between the mean plane of the indole ring system and the phenyl-sulfonyl ring are 71.67?(13) and 71.95?(13)° in the two mol-ecules while the indole unit and the thiophene ring make dihedral angles of 54.91?(12) and 56.92?(13)° in the two molecules. The crystal packing is stabilized by weak C-H?? inter-actions.

SUBMITTER: Kamalakumar C

PROVIDER: S-EPMC3052024 | biostudies-literature | 2011 Feb

REPOSITORIES: biostudies-literature

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(1-Phenyl-sulfonyl-1H-indol-2-yl)(thio-phen-2-yl)methanone.

Kamalakumar C C Dhayalan V V Mohanakrishnan A K AK Balasubramanian V V Manivannan V V

Acta crystallographica. Section E, Structure reports online 20110226 Pt 3

The crystal studied of the title compound, C(19)H(13)NO(3)S(2), was found to be a non-merohedral twin with a domain ratio of 0.877 (3):0.123 (3). There are two independent mol-ecules in the asymmetric unit. The dihedral angles between the mean plane of the indole ring system and the phenyl-sulfonyl ring are 71.67 (13) and 71.95 (13)° in the two mol-ecules while the indole unit and the thiophene ring make dihedral angles of 54.91 (12) and 56.92 (13)° in the two molecules. The crystal packing is s ...[more]

PMID: 21522480

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