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2,3-Dibromo-3-(5-nitro-2-fur-yl)-1-phenyl-propan-1-one.

ABSTRACT: In the title compound, C(13)H(9)Br(2)NO(4), the phenyl and 2-nitro-furan rings are linked by a 2,3-dibromo-propanal group, six atoms of which, including a furyl C atom, are disordered over two positions with a site-occupancy ratio of 0.733?(11):0.267?(11). The dihedral angle between the furan [maximum deviation = 0.028?(4)?Å] and phenyl rings in the major component is 16.9?(3)°. In the minor component, the corresponding values are 0.87?(4)?Å and 23.3?(5)°. In the crystal, inter-molecular C-H?O hydrogen bonds link the mol-ecules into two-dimensional arrays parallel to the ab plane.

SUBMITTER: Shahani T

PROVIDER: S-EPMC3052152 | biostudies-literature | 2011 Feb

REPOSITORIES: biostudies-literature

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2,3-Dibromo-3-(5-nitro-2-fur-yl)-1-phenyl-propan-1-one.

Shahani Tara T Fun Hoong-Kun HK Nithinchandra Kalluraya Balakrishna B

Acta crystallographica. Section E, Structure reports online 20110202 Pt 3

In the title compound, C(13)H(9)Br(2)NO(4), the phenyl and 2-nitro-furan rings are linked by a 2,3-dibromo-propanal group, six atoms of which, including a furyl C atom, are disordered over two positions with a site-occupancy ratio of 0.733 (11):0.267 (11). The dihedral angle between the furan [maximum deviation = 0.028 (4) Å] and phenyl rings in the major component is 16.9 (3)°. In the minor component, the corresponding values are 0.87 (4) Å and 23.3 (5)°. In the crystal, inter-molecular C-H⋯O h ...[more]

PMID: 21522313

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