Thermal stability of functionalized carbon nanotubes studied by in-situ transmission electron microscopy.
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ABSTRACT: The thermal stability of funtionalized carbon nanotubes (CNTs) has been studied experimentally by direct in-situ observations using a heating stage in a transmission electron microscope, from room temperature (RT) to about 1000 °C. It was found that the thermal stability of the functionalized CNTs was significantly reduced during the in-situ heating process. Their average diameter dramatically expanded from RT to about 500 °C, and then tended to be stable until about 1000 °C. The X-ray energy dispersive spectroscopy analysis suggested that the diameter expansion was associated with coalescence of the carbon structure instead of deposition with additional foreign elements during the heating process.
SUBMITTER: Luo Z
PROVIDER: S-EPMC3182121 | biostudies-literature | 2011 Sep
REPOSITORIES: biostudies-literature
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