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2-Cyano-N'-(5-hy-droxy-2-nitro-benzyl-idene)acetohydrazide monohydrate.

ABSTRACT: The title compound, C(10)H(8)N(4)O(4)·H(2)O, was obtained by the reaction of 5-hy-droxy-2-nitro-benzaldehyde with cyano-acetohydrazide in methanol. The non-H atoms of the hydrazone molecule are approximately coplanar, with a mean deviation from the least-squares plane of 0.056?Å. In the crystal, mol-ecules are linked by N-H?O, O-H?N and O-H?O hydrogen bonds, generating a three-dimensional network.

SUBMITTER: Li H

PROVIDER: S-EPMC3213457 | biostudies-literature | 2011 Aug

REPOSITORIES: biostudies-literature

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2-Cyano-N'-(5-hy-droxy-2-nitro-benzyl-idene)acetohydrazide monohydrate.

Li Hongbo H Ni Xiaocheng X

Acta crystallographica. Section E, Structure reports online 20110709 Pt 8

The title compound, C(10)H(8)N(4)O(4)·H(2)O, was obtained by the reaction of 5-hy-droxy-2-nitro-benzaldehyde with cyano-acetohydrazide in methanol. The non-H atoms of the hydrazone molecule are approximately coplanar, with a mean deviation from the least-squares plane of 0.056 Å. In the crystal, mol-ecules are linked by N-H⋯O, O-H⋯N and O-H⋯O hydrogen bonds, generating a three-dimensional network. ...[more]

PMID: 22091036

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