Unknown

Dataset Information

0

Rac-7-[(2E)-But-2-eno-yl]-13-chloro-N-cyclo-hexyl-7,8-dihydro-5H-isochromeno[4,3-c]phenanthridine-8-carboxamide.


ABSTRACT: In the title compound, C(31)H(29)ClN(2)O(3), the two heterocyclic rings, belonging to a system of five condensed rings, adopt conformations intermediate between twist-boat and sofa. The secondary amide group is involved in a weak intramolecular N-H?N hydrogen bond. In the crystal, molecules are linked by pairs of C-H?Cl hydrogen bonds to form inversion dimers. These dimers are linked via a C-H?O interaction to form chains propagating along the b-axis direction.

SUBMITTER: Ye N 

PROVIDER: S-EPMC3295516 | biostudies-literature | 2012 Mar

REPOSITORIES: biostudies-literature

altmetric image

Publications

rac-7-[(2E)-But-2-eno-yl]-13-chloro-N-cyclo-hexyl-7,8-dihydro-5H-isochromeno[4,3-c]phenanthridine-8-carboxamide.

Ye Ning N   Wu Jin-Long JL  

Acta crystallographica. Section E, Structure reports online 20120217 Pt 3


In the title compound, C(31)H(29)ClN(2)O(3), the two heterocyclic rings, belonging to a system of five condensed rings, adopt conformations intermediate between twist-boat and sofa. The secondary amide group is involved in a weak intramolecular N-H⋯N hydrogen bond. In the crystal, molecules are linked by pairs of C-H⋯Cl hydrogen bonds to form inversion dimers. These dimers are linked via a C-H⋯O interaction to form chains propagating along the b-axis direction. ...[more]

Similar Datasets

| S-EPMC6150310 | biostudies-literature
| S-EPMC6273168 | biostudies-literature
| S-EPMC3709772 | biostudies-literature
| S-EPMC2977510 | biostudies-literature
| S-EPMC3151951 | biostudies-literature
| S-EPMC2961529 | biostudies-literature
| S-EPMC2971955 | biostudies-literature
| S-EPMC2979018 | biostudies-literature
| S-EPMC6393703 | biostudies-literature
| S-EPMC6268426 | biostudies-literature