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(E)-4-Amino-N-(1,2-dihydro-pyridin-2-yl-idene)benzene-sulfonamide nitro-methane monosolvate.

ABSTRACT: In the title solvate, C(11)H(11)N(3)O(2)S·CH(3)NO(2), the dihedral angle between the benzene ring and the N-containing ring is 85.94 (11)°, and an approximate V shape arises for the sulfonamide mol-ecule. In the crystal, N-H⋯O and N-H⋯N hydrogen bonds and weak C-H⋯O inter-actions link the sulfonamide mol-ecules into a three-dimensional network. The nitro-methane solvent mol-ecules are located in the inter-stitial sites in the sulfonamide network.

SUBMITTER: Ghorab MM

PROVIDER: S-EPMC3343993 | biostudies-literature | 2012 Apr

REPOSITORIES: biostudies-literature

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(E)-4-Amino-N-(1,2-dihydro-pyridin-2-yl-idene)benzene-sulfonamide nitro-methane monosolvate.

Ghorab Mostafa M MM Al-Said Mansour S MS Ghabbour Hazem A HA Chantrapromma Suchada S Fun Hoong-Kun HK

Acta crystallographica. Section E, Structure reports online 20120310 Pt 4

In the title solvate, C(11)H(11)N(3)O(2)S·CH(3)NO(2), the dihedral angle between the benzene ring and the N-containing ring is 85.94 (11)°, and an approximate V shape arises for the sulfonamide mol-ecule. In the crystal, N-H⋯O and N-H⋯N hydrogen bonds and weak C-H⋯O inter-actions link the sulfonamide mol-ecules into a three-dimensional network. The nitro-methane solvent mol-ecules are located in the inter-stitial sites in the sulfonamide network. ...[more]

PMID: 22589902

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