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N-(4-Chloro-phen-yl)-4-meth-oxy-3-(propanamido)-benzamide cyclo-hexane hemisolvate.

ABSTRACT: The title compound, C(17)H(17)ClN(2)O(3)·0.5C(6)H(12), was prepared by the condensation reaction of 4-meth-oxy-3-(propanamido)-benzoic acid with 4-chloro-aniline. The Cl atom, the propionyl CH(3) group and the cyclo-hexyl CH(2) group are disordered over two sets of sites of equal occupancy in both mol-ecules. The cyclo-hexane solvent mol-ecule is disordered over two orientations which were modelled with relative occupancies of 0.484?(4) and 0.516?(4). In the crystal, there are a number of N-H?O hydrogen bonds, forming layers perpendicular to (001).

SUBMITTER: Zhong Z

PROVIDER: S-EPMC3344590 | biostudies-literature | 2012 May

REPOSITORIES: biostudies-literature

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N-(4-Chloro-phen-yl)-4-meth-oxy-3-(propanamido)-benzamide cyclo-hexane hemisolvate.

Zhong Zhaojin Z Li Zhuorong Z Gong Ningbo N Li Yanping Y

Acta crystallographica. Section E, Structure reports online 20120421 Pt 5

The title compound, C(17)H(17)ClN(2)O(3)·0.5C(6)H(12), was prepared by the condensation reaction of 4-meth-oxy-3-(propanamido)-benzoic acid with 4-chloro-aniline. The Cl atom, the propionyl CH(3) group and the cyclo-hexyl CH(2) group are disordered over two sets of sites of equal occupancy in both mol-ecules. The cyclo-hexane solvent mol-ecule is disordered over two orientations which were modelled with relative occupancies of 0.484 (4) and 0.516 (4). In the crystal, there are a number of N-H⋯O ...[more]

PMID: 22590352

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