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A co-crystal of 3-(3,5-dinitro-benzo-yl)-1,1-dimethyl-thio-urea and N,N-dimethyl-3,5-dinitro-benzamide.

ABSTRACT: In the title compound, C(10)H(10)N(4)O(5)S·C(9)H(9)N(3)O(5), the amide groups of 3-(3,5-dinitro-benzo-yl)-1,1-dimethyl-thio-urea and N,N-dimethyl-3,5-dinitro-benzamide mol-ecules are oriented at dihedral angles of 39.13?(8) and 55.97?(11)°, respectively, to the attached benzene rings. In the crystal, the two mol-ecules are linked by an N-H?O hydrogen bond. Weak C-H?O link the mol-ecules into a sheet parallel to the bc plane. C-H?S inter-actions also occur.

SUBMITTER: Saeed S 

PROVIDER: S-EPMC3515214 | biostudies-literature | 2012 Nov

REPOSITORIES: biostudies-literature

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A co-crystal of 3-(3,5-dinitro-benzo-yl)-1,1-dimethyl-thio-urea and N,N-dimethyl-3,5-dinitro-benzamide.

Saeed Sohail S   Rashid Naghmana N   Butcher Ray J RJ   Oztürk Yildirim Sema S   Hussain Rizwan R  

Acta crystallographica. Section E, Structure reports online 20121013 Pt 11

In the title compound, C(10)H(10)N(4)O(5)S·C(9)H(9)N(3)O(5), the amide groups of 3-(3,5-dinitro-benzo-yl)-1,1-dimethyl-thio-urea and N,N-dimethyl-3,5-dinitro-benzamide mol-ecules are oriented at dihedral angles of 39.13 (8) and 55.97 (11)°, respectively, to the attached benzene rings. In the crystal, the two mol-ecules are linked by an N-H⋯O hydrogen bond. Weak C-H⋯O link the mol-ecules into a sheet parallel to the bc plane. C-H⋯S inter-actions also occur. ...[more]

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