Unknown

Dataset Information

0

3-Hy-droxy-2-meth-oxy-benzamide.

ABSTRACT: The crystal structure of the title compound, C8H9NO3, features centrosymmetric dimers with two amide groups inter-connected by a pair of almost linear N-H?O hydrogen bonds. Through inter-molecular O-H?O inter-actions between phenolic hy-droxy groups and carbonyl O atoms, these dimers are assembled into undulating hydrogen-bonded layers parallel to the [101] plane. Additionally, the anti-H(-N) atom of the primary amide group forms an intra-molecular hydrogen bond to the O atom of the meth-oxy group. The amide group froms a dihedral angle of 12.6?(1)° with the phenyl ring.

SUBMITTER: Wilbrand S 

PROVIDER: S-EPMC3589065 | biostudies-literature | 2012 Dec

REPOSITORIES: biostudies-literature

Json Xml
altmetric image

Publications

3-Hy-droxy-2-meth-oxy-benzamide.

Wilbrand Sabine S   Neis Christian C   Hegetschweiler Kaspar K  

Acta crystallographica. Section E, Structure reports online 20121130 Pt 12

The crystal structure of the title compound, C8H9NO3, features centrosymmetric dimers with two amide groups inter-connected by a pair of almost linear N-H⋯O hydrogen bonds. Through inter-molecular O-H⋯O inter-actions between phenolic hy-droxy groups and carbonyl O atoms, these dimers are assembled into undulating hydrogen-bonded layers parallel to the [101] plane. Additionally, the anti-H(-N) atom of the primary amide group forms an intra-molecular hydrogen bond to the O atom of the meth-oxy gro  ...[more]

Similar Datasets

Unknown N-(4-Hy-droxy-phen-yl)-3,4,5-trimeth-oxy-benzamide.
| S-EPMC3247600 | biostudies-literature
Unknown 4-(5-Hy-droxy-meth-yl-2-meth-oxy-phen-oxy)benzoic acid.
| S-EPMC3089302 | biostudies-literature
Unknown (E)-4-Hy-droxy-N'-(3-hy-droxy-4-meth-oxy-benzyl-idene)benzohydrazide.
| S-EPMC3201407 | biostudies-literature
Unknown (E)-4-Hy-droxy-N'-(4-hy-droxy-3-meth-oxy-benzyl-idene)benzohydrazide.
| S-EPMC3011781 | biostudies-literature
Unknown (E)-4-Hy-droxy-N'-(2-hy-droxy-4-meth-oxy-benzyl-idene)benzohydrazide.
| S-EPMC3394058 | biostudies-literature
Unknown (E)-N'-(3-Hy-droxy-4-meth-oxy-benzyl-idene)-4-meth-oxy-benzohydrazide.
| S-EPMC3239014 | biostudies-literature
Unknown 5,6,7-Trichloro-2-meth-oxy-8-hy-droxy-quinoline.
| S-EPMC3089234 | biostudies-literature
Unknown 5-Hy-droxy-3,4',6,7-tetra-meth-oxy-flavone.
| S-EPMC3201397 | biostudies-literature
Unknown 2-[Hy-droxy(2-meth-oxy-phenyl)methyl]acrylonitrile.
| S-EPMC3414923 | biostudies-literature
Unknown 4-Hy-droxy-3-meth-oxy-benzaldehyde thio-semicarbazone.
| S-EPMC3885096 | biostudies-literature