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2-(2-Chloro-phen-yl)-N-cyclo-hexyl-2-oxoacetamide.

ABSTRACT: In the title compound, C14H16ClNO2, the cyclo-hexyl ring has a chair conformation. The dihedral angle between the benzene ring and the mean plane of the four planar C atoms of the cyclo-hexyl ring is 45.2?(3)°. The two carbonyl groups are trans to one another, with an O=C-C=O torsion angle of -137.1?(3)°. In the crystal, mol-ecules are linked by N-H?O hydrogen bonds forming chains propagating along [001]. A region of disordered electron density, situated near the unit-cell corners, was treated using the SQUEEZE routine in PLATON [Spek (2009 ?). Acta Cryst. D65, 148-155]. It gave a solvent-accessible void of ca 400?Å(3) for only 21 electrons. It is probably due to traces of the solvent of crystallization and was not taken into account during structure refinement.

SUBMITTER: Jin XD 

PROVIDER: S-EPMC3629535 | biostudies-literature | 2013 Apr

REPOSITORIES: biostudies-literature

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2-(2-Chloro-phen-yl)-N-cyclo-hexyl-2-oxoacetamide.

Jin Xiu-Dan XD   Wu Jin-Long JL  

Acta crystallographica. Section E, Structure reports online 20130309 Pt 4

In the title compound, C14H16ClNO2, the cyclo-hexyl ring has a chair conformation. The dihedral angle between the benzene ring and the mean plane of the four planar C atoms of the cyclo-hexyl ring is 45.2 (3)°. The two carbonyl groups are trans to one another, with an O=C-C=O torsion angle of -137.1 (3)°. In the crystal, mol-ecules are linked by N-H⋯O hydrogen bonds forming chains propagating along [001]. A region of disordered electron density, situated near the unit-cell corners, was treated u  ...[more]

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