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2-(Benzyl-carbamo-yl)nicotinic acid.

ABSTRACT: In the title compound, C14H12N2O3, the pyridine ring is twisted with respect to the phenyl ring and the carb-oxy-lic acid group at angles of 37.1?(5) and 8.1?(3)°, respectively; the phenyl ring forms a dihedral angle of 41.4?(1)° with the mean plane of the C-NH-C=O fragment. An intra-molecular O-H?O hydrogen bond occurs between the carb-oxy-lic acid and carbonyl groups. In the crystal, N-H?O hydrogen bonds link mol-ecules into a supra-molecular chain running along the a-axis direction.

SUBMITTER: Mao YC

PROVIDER: S-EPMC3790388 | biostudies-literature | 2013

REPOSITORIES: biostudies-literature

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2-(Benzyl-carbamo-yl)nicotinic acid.

Mao Yan-Cao YC Wu Hao H Shan Jin-Jun JJ Yan Ke K

Acta crystallographica. Section E, Structure reports online 20130907 Pt 10

In the title compound, C14H12N2O3, the pyridine ring is twisted with respect to the phenyl ring and the carb-oxy-lic acid group at angles of 37.1 (5) and 8.1 (3)°, respectively; the phenyl ring forms a dihedral angle of 41.4 (1)° with the mean plane of the C-NH-C=O fragment. An intra-molecular O-H⋯O hydrogen bond occurs between the carb-oxy-lic acid and carbonyl groups. In the crystal, N-H⋯O hydrogen bonds link mol-ecules into a supra-molecular chain running along the a-axis direction. ...[more]

PMID: 24098210

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