Unknown

Dataset Information

0

3,14-Diethyl-2,13-di-aza-6,17-diazonia-tri-cyclo-[16.4.0.0(7,12)]docosane dichloride tetra-hydrate from synchrotron radiation.

ABSTRACT: The asymmetric unit of title hydrated salt, C22H46N4 (2+)·2Cl(-)·4H2O, comprises half a centrosymmetric dication, one Cl(-) anion and two water mol-ecules of crystallization. The structure determination reveals that protonation has occurred at diagonally opposite amine N atoms, and that the dication features intra-molecular N-H⋯N hydrogen bonds. In the crystal, a three-dimensional artchitecture is formed by O-H⋯Cl/N and N-H⋯Cl/O hydrogen bonds.

SUBMITTER: Moon D 

PROVIDER: S-EPMC3884294 | biostudies-literature | 2013 Oct

REPOSITORIES: biostudies-literature

Json Xml
altmetric image

Publications

3,14-Diethyl-2,13-di-aza-6,17-diazonia-tri-cyclo-[16.4.0.0(7,12)]docosane dichloride tetra-hydrate from synchrotron radiation.

Moon Dohyun D   Subhan Md Abdus MA   Choi Jong-Ha JH  

Acta crystallographica. Section E, Structure reports online 20131009 Pt 11

The asymmetric unit of title hydrated salt, C22H46N4 (2+)·2Cl(-)·4H2O, comprises half a centrosymmetric dication, one Cl(-) anion and two water mol-ecules of crystallization. The structure determination reveals that protonation has occurred at diagonally opposite amine N atoms, and that the dication features intra-molecular N-H⋯N hydrogen bonds. In the crystal, a three-dimensional artchitecture is formed by O-H⋯Cl/N and N-H⋯Cl/O hydrogen bonds. ...[more]

Similar Datasets

Unknown Crystal structure of 3,14-diethyl-2,13-di-aza-6,17-diazo-niatri-cyclo-[16.4.0.0<sup>7,12</sup>]docosane dinitrate dihydrate from synchrotron X-ray data.
| S-EPMC6658972 | biostudies-literature
Unknown Crystal structure of 3,14-dimethyl-2,13-di-aza-6,17-diazo-niatri-cyclo-[16.4.0.0<sup>7,12</sup>]docosane bis-(per-chlorate) from synchrotron X-ray data.
| S-EPMC8100260 | biostudies-literature
Unknown Crystal structure of 3,14-diethyl-2,6,13,17-tetra-azoniatri-cyclo-[16.4.0.0<sup>7,12</sup>]docosane tetra-chloride tetra-hydrate from synchrotron X-ray data.
| S-EPMC7869539 | biostudies-literature
Unknown Crystal structure of 3,14-dimethyl-2,6,13,17-tetra-azoniatri-cyclo-[16.4.0.0<sup>7,12</sup>]docosane tetra-chloride tetra-hydrate from synchrotron X-ray data.
| S-EPMC6072991 | biostudies-literature
Unknown Crystal structure of [2,13-bis-(acetamido)-5,16-dimethyl-2,6,13,17-tetra-aza-tri-cyclo-[16.4.0.0<sup>7,12</sup>]docosane-κ<sup>4</sup><i>N</i>]silver(II) dinitrate from synchrotron X-ray data.
| S-EPMC5946968 | biostudies-literature
Unknown Crystal structure of di-aqua-(3,14-diethyl-2,6,13,17-tetra-aza-tri-cyclo-[16.4.0.0<sup>7,12</sup>]docosa-ne)copper(II) (3,14-diethyl-2,6,13,17-tetra-aza-tri-cyclo[16.4.0.0<sup>7,12</sup>]docosa-ne)copper(II) tetra-bromide dihydrate, [Cu(C<sub>22</sub>H<sub>44</sub>N<sub>4</sub>)(H<sub>2</sub>O)<sub>2</sub>][Cu(C<sub>22</sub>H<sub>44</sub>N<sub>4</sub>)]Br<sub>4</sub>·2H<sub>2</sub>O.
| S-EPMC8183443 | biostudies-literature
Unknown (S)-2-Methylpiperazinediium dichloride 0.42-hydrate.
| S-EPMC2961261 | biostudies-literature
Unknown Hexaaqua-zinc(II) dichloride bis-(hexa-methyl-enetetramine) tetra-hydrate.
| S-EPMC2960671 | biostudies-literature
Unknown Diethyl 7,8,18,19-tetra-methyl-2,13-dioxo-hexa-cyclo-[10.10.2.0.0.0.0]tetra-cosa-5,7,9,16,18,20-hexa-ene-23,24-dicarboxyl-ate.
| S-EPMC3006902 | biostudies-literature
Unknown 6,6'-Dimethyl-2,2'-[oxalylbis(aza-nedi-yl)]dipyridinium dichloride acetonitrile solvate.
| S-EPMC3007829 | biostudies-literature