Unknown

Dataset Information

0

1,5-Bis(2-hy-droxy-3-meth-oxy-benzyl-idene)carbonohydrazide methanol 0.47-solvate.

ABSTRACT: In the title compound, C17H18N4O5·0.47CH3OH, the virtually planar (r.m.s. deviation = 0.128?Å) carbonohydrazide mol-ecule is located on a twofold axis and conformation of its C=N bonds is E. There are short intra-molecular O-H?N hydrogen bonds between the hy-droxy groups and hydrazide N atoms. In the crystal, bifurcated N-H?(O,O) hydrogen bonds assemble the carbonohydrazide mol-ecules into a three-dimensional network. There are C 2 symmetric voids in this network, 47% of which are occupied by disordered methanol mol-ecules.

SUBMITTER: Sow MM 

PROVIDER: S-EPMC3998575 | biostudies-literature | 2014 Apr

REPOSITORIES: biostudies-literature

Json Xml
altmetric image

Publications

1,5-Bis(2-hy-droxy-3-meth-oxy-benzyl-idene)carbonohydrazide methanol 0.47-solvate.

Sow Mouhamadou Moustapha MM   Diouf Ousmane O   Seck Matar M   Barry Aliou Hamady AH   Gaye Mohamed M  

Acta crystallographica. Section E, Structure reports online 20140312 Pt 4

In the title compound, C17H18N4O5·0.47CH3OH, the virtually planar (r.m.s. deviation = 0.128 Å) carbonohydrazide mol-ecule is located on a twofold axis and conformation of its C=N bonds is E. There are short intra-molecular O-H⋯N hydrogen bonds between the hy-droxy groups and hydrazide N atoms. In the crystal, bifurcated N-H⋯(O,O) hydrogen bonds assemble the carbonohydrazide mol-ecules into a three-dimensional network. There are C 2 symmetric voids in this network, 47% of which are occupied by di  ...[more]

Similar Datasets

Unknown 1,5-Bis(2-meth-oxy-benzyl-idene)thio-carbonohydrazide methanol monosolvate.
| S-EPMC3770410 | biostudies-literature
Unknown 1,5-Bis(4-meth-oxy-benzyl-idene)thio-carbonohydrazide methanol monosolvate.
| S-EPMC3213573 | biostudies-literature
Unknown (E)-N'-(5-Bromo-2-hy-droxy-benzyl-idene)-4-hy-droxy-3-meth-oxy-benzohydrazide methanol solvate.
| S-EPMC3006942 | biostudies-literature
Unknown 4-Chloro-N'-(2-hy-droxy-4-meth-oxy-benzyl-idene)benzohydrazide methanol monosolvate.
| S-EPMC3247565 | biostudies-literature
Unknown 4-Dimethyl-amino-N'-(2-hy-droxy-4-meth-oxy-benzyl-idene)benzohydrazide methanol monosolvate.
| S-EPMC3470357 | biostudies-literature
Unknown (E)-4-Hy-droxy-N'-(3-hy-droxy-4-meth-oxy-benzyl-idene)benzohydrazide.
| S-EPMC3201407 | biostudies-literature
Unknown (E)-4-Hy-droxy-N'-(2-hy-droxy-4-meth-oxy-benzyl-idene)benzohydrazide.
| S-EPMC3394058 | biostudies-literature
Unknown (E)-4-Hy-droxy-N'-(4-hy-droxy-3-meth-oxy-benzyl-idene)benzohydrazide.
| S-EPMC3011781 | biostudies-literature
Unknown N'-(4-Hy-droxy-benzyl-idene)-3-meth-oxy-benzohydrazide.
| S-EPMC3274989 | biostudies-literature
Unknown (E)-N'-(3-Hy-droxy-4-meth-oxy-benzyl-idene)-4-meth-oxy-benzohydrazide.
| S-EPMC3239014 | biostudies-literature