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N-(2-Nitro-phen-yl)thio-phene-2-carbox-amide.

ABSTRACT: The title compound, C11H8N2O3S, shows two mol-ecules per asymmetric unit, with the dihedral angles between the benzene and thio-phene rings of 13.53?(6) and 8.50?(5)° being a notable difference between them. An intra-molecular N-H?O hydrogen-bond in each mol-ecule generates an S(6) ring motif. The crystal packing shows no classical hydrogen bonds with the mol-ecules being packed to form weak C-H?O and C-H?S inter-actions leading to R 2 (2)(9) and R 4 (4)(25) rings which are edge-shared, giving layers parallel to (010).

SUBMITTER: Moreno-Fuquen R

PROVIDER: S-EPMC4011230 | biostudies-literature | 2014 May

REPOSITORIES: biostudies-literature

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N-(2-Nitro-phen-yl)thio-phene-2-carbox-amide.

Moreno-Fuquen Rodolfo R Azcárate Alexis A Kennedy Alan R AR

Acta crystallographica. Section E, Structure reports online 20140426 Pt 5

The title compound, C11H8N2O3S, shows two mol-ecules per asymmetric unit, with the dihedral angles between the benzene and thio-phene rings of 13.53 (6) and 8.50 (5)° being a notable difference between them. An intra-molecular N-H⋯O hydrogen-bond in each mol-ecule generates an S(6) ring motif. The crystal packing shows no classical hydrogen bonds with the mol-ecules being packed to form weak C-H⋯O and C-H⋯S inter-actions leading to R 2 (2)(9) and R 4 (4)(25) rings which are edge-shared, giving l ...[more]

PMID: 24860404

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