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1-(4-Chloro-butano-yl)-3-(3-chloro-phen-yl)thio-urea.

ABSTRACT: The two independent mol-ecules in the asymmetric unit of the title compound, C11H12Cl2N2OS, exhibit different conformations, with the benzene ring and the N2CS thio-urea group forming dihedral angles of 87.40?(18) and 69.42?(15)°. An intra-molecular N-H?O hydrogen bond is present in each mol-ecule. Two further N-H?O hydrogen bonds link the independent mol-ecules into a dimer. In the crystal, the dimers are linked by N-H?S and C-H?S hydrogen bonds, forming chains parallel to the c axis.

SUBMITTER: Abosadiya HM 

PROVIDER: S-EPMC4051110 | biostudies-literature | 2014 Jun

REPOSITORIES: biostudies-literature

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1-(4-Chloro-butano-yl)-3-(3-chloro-phen-yl)thio-urea.

Abosadiya Hamza M HM   Hasbullah Siti Aishah SA   Yamin Bohari M BM   Fadzil Adibatul H AH  

Acta crystallographica. Section E, Structure reports online 20140517 Pt 6

The two independent mol-ecules in the asymmetric unit of the title compound, C11H12Cl2N2OS, exhibit different conformations, with the benzene ring and the N2CS thio-urea group forming dihedral angles of 87.40 (18) and 69.42 (15)°. An intra-molecular N-H⋯O hydrogen bond is present in each mol-ecule. Two further N-H⋯O hydrogen bonds link the independent mol-ecules into a dimer. In the crystal, the dimers are linked by N-H⋯S and C-H⋯S hydrogen bonds, forming chains parallel to the c axis. ...[more]

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