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High saturation magnetization of ?-Fe2O3 nano-particles by a facile one-step synthesis approach.


ABSTRACT: We have demonstrated the synthesis of ?-Fe2O3 nano-particles through a facile and novel calcination process in the air. There is no pH regulation, gas atmosphere, additive, centrifugation or other complicated procedures during the preparing process. A detailed formation process of the nano-particles is proposed, and DMF as a polar solvent may slower the reaction process of calcination. The structures, morphologies, and magnetic properties of ?-Fe2O3 nano-particles were investigated systematically, and the pure ?-Fe2O3 nano-particles obtained at 200?°C display uniform morphology good magnetic property. The saturation magnetization of obtained pure ?-Fe2O3 is about 74?emu/g, which is comparable with bulk material (76?emu/g) and larger than other results. In addition, the photocatalytic activity for degradation of methylene blue is also studied, which shows proper photocatalytic activity.

SUBMITTER: Cao D 

PROVIDER: S-EPMC5007676 | biostudies-literature | 2016 Sep

REPOSITORIES: biostudies-literature

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High saturation magnetization of γ-Fe2O3 nano-particles by a facile one-step synthesis approach.

Cao Derang D   Li Hao H   Pan Lining L   Li Jianan J   Wang Xicheng X   Jing Panpan P   Cheng Xiaohong X   Wang Wenjie W   Wang Jianbo J   Liu Qingfang Q  

Scientific reports 20160901


We have demonstrated the synthesis of γ-Fe2O3 nano-particles through a facile and novel calcination process in the air. There is no pH regulation, gas atmosphere, additive, centrifugation or other complicated procedures during the preparing process. A detailed formation process of the nano-particles is proposed, and DMF as a polar solvent may slower the reaction process of calcination. The structures, morphologies, and magnetic properties of γ-Fe2O3 nano-particles were investigated systematicall  ...[more]

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