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Influence of Crystalline Admixtures on the Short-Term Behaviour of Mortars Exposed to Sulphuric Acid.

ABSTRACT: Using durable materials is a sustainable solution for extending the lifetime of constructions. The use of crystalline admixtures makes cementitious materials more durable. They plug pores, capillary tracts and microcracks, blocking the entrance of water due to the formation of crystals that prevent the penetration of liquids. The literature has covered the performance of these admixtures on concrete, but studies on mortars are still scarce. The aim of this study is to investigate the effect of an aggressive environment (sulphuric acid solution-3 wt%) on mortars produced with different percentages of a crystalline admixture (1%, 1.5% and 2% by weight of cement content). Physical and mechanical properties were studied after immersing the mortars in a H?SO? solution for 90 days. It was found that, after a 90-day sulphuric acid exposure, mortars with the crystalline admixture showed greater compressive strength than the control mortar, besides exhibiting lower mass loss. However, the crystalline admixture did not produce any significant effect on the capillary water absorption coefficient. In a nonaggressive environment, and in the short term, the crystalline admixture did not have a significant effect on the compressive strength, the capillary water absorption coefficient or the ultrasonic pulse velocity.

SUBMITTER: Garcia-Vera VE

PROVIDER: S-EPMC6337189 | biostudies-literature | 2018 Dec

REPOSITORIES: biostudies-literature

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Influence of Crystalline Admixtures on the Short-Term Behaviour of Mortars Exposed to Sulphuric Acid.

García-Vera Victoria Eugenia VE Tenza-Abril Antonio José AJ Saval José Miguel JM Lanzón Marcos M

Materials (Basel, Switzerland) 20181227 1

Using durable materials is a sustainable solution for extending the lifetime of constructions. The use of crystalline admixtures makes cementitious materials more durable. They plug pores, capillary tracts and microcracks, blocking the entrance of water due to the formation of crystals that prevent the penetration of liquids. The literature has covered the performance of these admixtures on concrete, but studies on mortars are still scarce. The aim of this study is to investigate the effect of a ...[more]

PMID: 30591624

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Project description:The durability of a cement-based material is mainly dependent on its permeability. Modifications of porosity, pore-structure and pore-connectivity could have significant impacts on permeability improvement, which eventually leads to more durable materials. One of the most efficient solutions in this regard is to use permeability reducing admixtures (PRA). Among these admixtures for those structures exposed to hydro-static pressure, crystalline waterproofing admixtures (CWA) have been serving in the construction industries for decades and according to ACI 212-chemical admixtures' report, it has proven its capability in permeability reduction and durability-enhancement. However, there is substantial research being done on its durability properties at the macro level but very limited information available regarding its microstructural features and chemical characteristics at the micro level. Hence, this paper presents one of the first reported attempts to characterize microstructural and chemical elements of hydration products for cementitious composites with CWA called K, P and X using Scanning Electron Microscopy (SEM). Backscattered SEM images taken from a polished-section of one CWA type-K-admixture were analyzed in ImageJ to obtain paste matrix porosity, indicating a lower value for the CWA-K mixture. X-ray analysis and SEM micrographs of polished sections were examined to identify chemical compositions based on atomic ratio plots and brightness differences in backscatter-SEM images. To detect chemical elements and the nature of formed crystals, the fractured surfaces of three different CWA mixtures were examined. Cementitious composites with K admixture indicated needle-like crystal formation-though different from ettringite; X and P admixtures showed sulfur peaks in Energy Dispersive Spectrum (EDS) spectra, like ettringite. SEM images and X-ray analyses of mixtures incorporating Portland Limestone Cement (PLC) indicated lower-than-average porosity but showed different Si/Ca and Al/Ca atomic ratios.

Dataset Information

Influence of Crystalline Admixtures on the Short-Term Behaviour of Mortars Exposed to Sulphuric Acid.

Publications

Influence of Crystalline Admixtures on the Short-Term Behaviour of Mortars Exposed to Sulphuric Acid.

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