Dataset Information

Data on yields, sugars and glycosidic-linkage analyses of coffee arabinogalactan and galactomannan mixtures and optimization of their microwave assisted extraction from spent coffee grounds.

ABSTRACT: The data presented here are related to the research paper entitled "Structural features of spent coffee grounds water-soluble polysaccharides: towards tailor-made microwave assisted extractions" [1]. Microwave assisted extraction conditions were applied to spent coffee grounds for recovery of polysaccharides, namely arabinogalactans and galactomannans. Following an experimental design testing temperature, time, and alkali conditions as influence factors during microwave assisted extraction, this article reports the response data for the total extracted mass, sugars yield (including arabinogalactans and galactomannans total content, and mass ratio), and structural features (including degree of polymerization and degree of branching) for each set of operating conditions. In addition, it provides gas chromatography-mass spectrometry (GC-MS) chromatograms (and respective GC-MS spectra) of arabinogalactan and galactomannan mixtures with different structural features corresponding to representative microwave treatment conditions.

SUBMITTER: Passos CP

PROVIDER: S-EPMC6514364 | biostudies-literature | 2019 Jun

REPOSITORIES: biostudies-literature

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Data on yields, sugars and glycosidic-linkage analyses of coffee arabinogalactan and galactomannan mixtures and optimization of their microwave assisted extraction from spent coffee grounds.

Passos Cláudia P CP Rudnitskaya Alisa A Neves José M M G C JMMGC Lopes Guido R GR Coimbra Manuel A MA

Data in brief 20190419

The data presented here are related to the research paper entitled "Structural features of spent coffee grounds water-soluble polysaccharides: towards tailor-made microwave assisted extractions" [1]. Microwave assisted extraction conditions were applied to spent coffee grounds for recovery of polysaccharides, namely arabinogalactans and galactomannans. Following an experimental design testing temperature, time, and alkali conditions as influence factors during microwave assisted extraction, this ...[more]

PMID: 31193029

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Project description:Torrefaction of biomass is a promising thermochemical pretreatment technique used to upgrade the properties of biomass to produce solid fuel with improved fuel properties. A comparative study of the effects of torrefaction temperatures (200, 250, and 300 °C) and residence times (0.5 and 1 h) on the quality of torrefied biomass samples derived from spent coffee grounds (SCG) and coffee husk (CH) were conducted. An increase in torrefaction temperature (200-300 °C) and residence time (0.5-1 h) for CH led to an improvement in the fixed carbon content (17.9-31.8 wt %), calorific value (18.3-25 MJ/kg), and carbon content (48.5-61.2 wt %). Similarly, the fixed carbon content, calorific value, and carbon content of SCG rose by 14.6-29 wt %, 22.3-30.3 MJ/kg, and 50-69.5 wt %, respectively, with increasing temperature and residence time. Moreover, torrefaction led to an improvement in the hydrophobicity and specific surface area of CH and SCG. The H/C and O/C atomic ratios for both CH- and SCG-derived torrefied biomass samples were in the range of 0.93-1.0 and 0.19-0.20, respectively. Moreover, a significant increase in volatile compound yield was observed at temperatures between 250 and 300 °C. Maximum volatile compound yields of 11.9 and 6.2 wt % were obtained for CH and SCG, respectively. A comprehensive torrefaction model for CH and SCG developed in Aspen Plus provided information on the mass and energy flows and the overall process energy efficiency. Based on the modeling results, it was observed that with increasing torrefaction temperature to 300 °C, the mass and energy yield values of the torrefied biomass samples declined remarkably (97.3% at 250 °C to 67.5% at 300 °C for CH and 96.7% at 250 °C to 75.1% at 300 °C for SCG). The SCG-derived torrefied biomass tested for CO2 adsorption at 25 °C had a comparatively higher adsorption capacity of 0.38 mmol/g owing to its better textural characteristics. SCG would need further thermal treatment or functionalization to tailor the surface properties to attract more CO2 molecules under a typical post-combustion scenario.

Dataset Information

Data on yields, sugars and glycosidic-linkage analyses of coffee arabinogalactan and galactomannan mixtures and optimization of their microwave assisted extraction from spent coffee grounds.

Publications

Data on yields, sugars and glycosidic-linkage analyses of coffee arabinogalactan and galactomannan mixtures and optimization of their microwave assisted extraction from spent coffee grounds.

Similar Datasets

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