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Surface characterization data for tethered polyacrylic acid layers synthesized on polysulfone surfaces.

ABSTRACT: The data presented are supplementary to an article [Kim et al., 2019] on synthesis and surface characterization of tethered polyacrylic acid (PAA) layers on polysulfone (PSf) film/membrane surfaces via atmospheric pressure plasma-induced graft polymerization (APPIGP). Data on surface characterization of the synthesized tethered PAA layers includes: AFM topographic surface images and height distributions of surface features, dry layer thickness, chain rupture length distributions determined via AFM based force spectroscopy (AFM-FS), in addition to measurements of water contact angles. Fouling propensity data for ultrafiltration of alginic acid as a model foulant are also provided for native and PAA grafted PSf ultrafiltration (UF) membranes.

SUBMITTER: Kim S

PROVIDER: S-EPMC6660637 | biostudies-literature | 2019 Apr

REPOSITORIES: biostudies-literature

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Surface characterization data for tethered polyacrylic acid layers synthesized on polysulfone surfaces.

Kim Soomin S Moses Kari J KJ Sharma Shivani S Bilal Muhammad M Cohen Yoram Y

Data in brief 20190307

The data presented are supplementary to an article [Kim et al., 2019] on synthesis and surface characterization of tethered polyacrylic acid (PAA) layers on polysulfone (PSf) film/membrane surfaces via atmospheric pressure plasma-induced graft polymerization (APPIGP). Data on surface characterization of the synthesized tethered PAA layers includes: AFM topographic surface images and height distributions of surface features, dry layer thickness, chain rupture length distributions determined via A ...[more]

PMID: 31372412

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Project description:This study deals with the development of antifouling ultrafiltration membranes based on polysulfone (PSF) for wastewater treatment and the concentration and purification of hemicellulose and lignin in the pulp and paper industry. The efficient simple and reproducible technique of PSF membrane modification to increase antifouling performance by simultaneous addition of triblock copolymer polyethylene glycol-polypropylene glycol-polyethylene glycol (Synperonic F108, Mn =14 × 103 g mol-1) to the casting solution and addition of polyacrylic acid (PAA, Mn = 250 × 103 g mol-1) to the coagulation bath is proposed for the first time. The effect of the PAA concentration in the aqueous solution on the PSF/Synperonic F108 membrane structure, surface characteristics, performance, and antifouling stability was investigated. PAA concentrations were varied from 0.35 to 2.0 wt.%. Membrane composition, structure, and topology were investigated by Fourier-transform infrared spectroscopy (FTIR), X-ray photoelectron spectroscopy (XPS), atomic force microscopy (AFM), and scanning electron microscopy (SEM). The addition of PAA into the coagulation bath was revealed to cause the formation of a thicker and denser selective layer with decreasing its pore size and porosity; according to the structural characterization, an interpolymer complex of the two additives was formed on the surface of the PSF membrane. Hydrophilicity of the membrane selective layer surface was shown to increase significantly. The selective layer surface charge was found to become more negative in comparison to the reference membrane. It was shown that PSF/Synperonic F108/PAA membranes are characterized by better antifouling performance in ultrafiltration of humic acid solution and thermomechanical pulp mill (ThMP) process water. Membrane modification with PAA results in higher ThMP process water flux, fouling recovery ratio, and hemicellulose and total lignin rejection compared to the reference PSF/Synperonic F108 membrane. This suggests the possibility of applying the developed membranes for hemicellulose concentration and purification.

Dataset Information

Surface characterization data for tethered polyacrylic acid layers synthesized on polysulfone surfaces.

Publications

Surface characterization data for tethered polyacrylic acid layers synthesized on polysulfone surfaces.

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