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Role of Cellulose Micro and Nano Crystals in Thin Film and Support Layer of Nanocomposite Membranes for Brackish Water Desalination.

ABSTRACT: Reverse osmosis is a major process that produces soft water from saline water, and its output represents the majority of the overall desalination plants production. Developing efficient membranes for this process is the aim of many research groups and companies. In this work, we studied the effect of adding cellulose micro crystals (CMCs) and cellulose nano crystals (CNCs) to the support layer and thin film nanocomposite (TFN) membrane on the desalination performance. SEM, TEM, ATR-FTIR, and contact angle measurements were used to characterize the membrane's properties; and membrane's performance were evaluated by water flux and NaCl rejection. Filling 2% of CNCs gel in the support layer improved the water flux by +40%, while salt rejection maintained almost the same, around 95%. However, no remarkable improvement was gained by adding CNCs gel to m-phenylenediamine (MPD) solution, which was used in TFN membrane preparation. Filling CMCs powder in TFN membrane led to a slight improvement in terms of water flux.

SUBMITTER: Kadhom M

PROVIDER: S-EPMC6723096 | biostudies-literature | 2019 Aug

REPOSITORIES: biostudies-literature

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Role of Cellulose Micro and Nano Crystals in Thin Film and Support Layer of Nanocomposite Membranes for Brackish Water Desalination.

Kadhom Mohammed M Albayati Noor N Salih Suhaib S Al-Furaiji Mustafa M Bayati Mohamed M Deng Baolin B

Membranes 20190815 8

Reverse osmosis is a major process that produces soft water from saline water, and its output represents the majority of the overall desalination plants production. Developing efficient membranes for this process is the aim of many research groups and companies. In this work, we studied the effect of adding cellulose micro crystals (CMCs) and cellulose nano crystals (CNCs) to the support layer and thin film nanocomposite (TFN) membrane on the desalination performance. SEM, TEM, ATR-FTIR, and con ...[more]

PMID: 31443233

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Project description:The separation of biomacromolecules, mainly proteins, plays a significant role in the pharmaceutical and food industries. Among the membranes' techniques, thin-film nanocomposite nanofiltration membranes are the best choice due to their high energy efficiency, excellent productivity, cost-effective and tuneable properties that have captured the attention of the efficient separation of biomacromolecules, especially from the industrial perspective. The present work directs the efficient separation study of proteins, namely, lysozyme, trypsin, pepsin, bovine serum albumin (BSA), and cephalexin, using a thin-film nanocomposite membrane integrated with Arg-MMT (arginine-montmorillonite) clay nanoparticles. The surface morphology and cross-section images of the TFN membranes were studied using a field emission scanning electron microscope (FE-SEM) and a high-resolution transmission electron microscope (HR-TEM). The thermal stability and hydrophilicity of the membranes were examined using thermogravimetric analysis (TGA) and contact angle, respectively. The surface chemistry of the selective layer has different functional groups that were analyzed using FTIR spectroscopy. The performance of the membranes was studied at different trans-membrane pressures and permeation times. The effect of monomer concentration on the separation performance of the membranes was also studied at different permeation times. The membranes' antibacterial activity was evaluated using the Muller-Hinton disk diffusion method using gram-negative Escherichia coli (E. coli) and gram-positive Staphylococcus aureus (S. aureus) bacteria. The highest rejection was achieved for BSA up to 98.92 ± 1%, and the highest permeation was obtained against lysozyme feed solution up to 26 L m-2 h-1 at 5 bar pressure. The membrane also illustrated excellent rejection of cephalexin antibiotics with a rejection of 98.17 ± 1.75% and a permeation flux of 26.14 L m-2 h-1. The antifouling study performed for the membranes exhibited a flux recovery ratio of 86.48%. The fabricated thin-film nanocomposite membrane demonstrated a good alternative for the separation of biomacromolecules and has the potential to be used in different sectors of industry, especially the pharmaceutical and food industry.

Dataset Information

Role of Cellulose Micro and Nano Crystals in Thin Film and Support Layer of Nanocomposite Membranes for Brackish Water Desalination.

Publications

Role of Cellulose Micro and Nano Crystals in Thin Film and Support Layer of Nanocomposite Membranes for Brackish Water Desalination.

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