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First Synthesis of (-)-Altenuene-D3 Suitable as Internal Standard for Isotope Dilution Mass Spectrometry.


ABSTRACT: Metabolites from Alternaria fungi exhibit a variety of biological properties such as phytotoxic, cytotoxic, or antimicrobial activity. Optimization of a literature procedure culminated in an efficient total synthesis of (-)-altenuene as well as a stable isotope-labeled derivative suitable for implementation in a LC-MS/MS method for mycotoxin analysis.

SUBMITTER: Sebald MA 

PROVIDER: S-EPMC6943508 | biostudies-literature | 2019 Dec

REPOSITORIES: biostudies-literature

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First Synthesis of <i>(-)</i>-Altenuene-D<sub>3</sub> Suitable as Internal Standard for Isotope Dilution Mass Spectrometry.

Sebald Michael A MA   Gebauer Julian J   Sommerfeld Thomas T   Koch Matthias M  

Molecules (Basel, Switzerland) 20191212 24


Metabolites from <i>Alternaria</i> fungi exhibit a variety of biological properties such as phytotoxic, cytotoxic, or antimicrobial activity. Optimization of a literature procedure culminated in an efficient total synthesis of <i>(-)</i>-altenuene as well as a stable isotope-labeled derivative suitable for implementation in a LC-MS/MS method for mycotoxin analysis. ...[more]

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