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ABSTRACT:
SUBMITTER: Albrecht R
PROVIDER: S-EPMC7534229 | biostudies-literature | 2020 Oct
REPOSITORIES: biostudies-literature
Acta crystallographica. Section E, Crystallographic communications 20200911 Pt 10
Single-crystals of thallium(I) iodide oxide Tl<sub>3</sub>IO were obtained as by-product in a hydro-flux synthesis at 473 K for 10 h. A potassium hydroxide hydro-flux with a water-base molar ratio of 1.6 and the starting materials TlNO<sub>3</sub>, RhI<sub>3</sub> and Ba(NO<sub>3</sub>)<sub>2</sub> was used, resulting in a few black needle-shaped crystals. X-ray diffraction on a single-crystal revealed the hexa-gonal space group <i>P</i>6<sub>3</sub>/<i>mmc</i> (No. 194) with lattice parameters ...[more]