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X-ray diffraction and thermoanalytical datasets of precursors of the Gd6UO12-δ phase processed by combined mechanochemical-thermal routes.

ABSTRACT: The datasets presented here are related to the research paper entitled "Disordered Gd6UO12-δ with the cation antisite defects prepared by a combined mechanochemical-thermal method"[1]. The datasets complement the findings [1] on the effect of the combined mechanochemical-thermal processing of the stoichiometric mixture of solid precursors (3Gd2O3 + UO2) on the formation of Gd6UO12-δ phase. In this article, we provide (i) X-ray diffraction (XRD) data of the 3Gd2O3 + UO2 mixture milled for 12 h, (ii) the refined XRD data of the non-milled 3Gd2O3 + UO2 mixture after annealing at 1282 °C for 3 h in air, and (iii) the thermogravimetric and differential thermal analysis (TG-DTA) data for non-milled and mechanically preactivated 3Gd2O3 + UO2 mixture measured in air at a heat rate of 10 K/min.

SUBMITTER: Darin G 

PROVIDER: S-EPMC8027681 | biostudies-literature | 2021 Apr

REPOSITORIES: biostudies-literature

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X-ray diffraction and thermoanalytical datasets of precursors of the Gd<sub>6</sub>UO<sub>12-δ</sub> phase processed by combined mechanochemical-thermal routes.

Darin Gaspar G   Imakuma Kengo K   Santiago Rafael Trautwein RT   Da Silva Klebson Lucenildo KL   Cótica Luiz Fernardo LF   Fabián Martin M   Valíček Jan J   Hahn Horst H   Šepelák Vladimír V  

Data in brief 20210318

The datasets presented here are related to the research paper entitled <i>"Disordered</i> Gd<sub>6</sub>UO<sub>12-δ</sub> <i>with the cation antisite defects prepared by a combined mechanochemical-thermal method"</i>[1]. The datasets complement the findings [1] on the effect of the combined mechanochemical-thermal processing of the stoichiometric mixture of solid precursors (3Gd<sub>2</sub>O<sub>3</sub> + UO<sub>2</sub>) on the formation of Gd<sub>6</sub>UO<sub>12-δ</sub> phase. In this article,  ...[more]

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