Effect of Drying on the Fabrication of MgAl Layered Double Hydroxides.

ABSTRACT: This study aimed to evaluate the synthesis of MgAl/LDH from the drying process perspective, evaluating the influence of temperature (75-90 °C) and time (16-20 h) in the drying process. The synthesis was performed, maintaining a ratio of 2:1 of Mg/Al, and the drying was conducted according to a 2² experimental design: four axial points and three repetitions at the central point. The surface area and pore diameter ranged from 4.09 to 18.55 m²/g and 12.50 to 24.46 nm. Fourier transform infrared (FTIR) analysis indicated the drying-caused variation of the LDH typical bands intensities. Scanning electron microscopy (SEM) images showed the tendency of the increase of agglomeration with the temperature elevation. The drying parameters' influence was evident for X-ray diffrac

SUBMITTER: Silva Neto LD 

PROVIDER: S-EPMC8388087 | biostudies-literature | 2021 Aug

REPOSITORIES: biostudies-literature