Dataset Information

Inorganically modified particles FeAl-LDH@SiO₂ as reinforcement in poly (methyl) methacrylate matrix composite.

ABSTRACT: Silica particles were obtained from rice husk to which layered double hydroxide particles were deposited (weight ratio 1 : 1). Fe²⁺-Al³⁺ layered double hydroxides (FeAl-LDH) were synthesized by co-precipitation with ratios Fe : Al of 3 : 1 in the presence of SiO₂ particles from the rice husk. Characterization of the synthesized FeAl-LDH@SiO₂ particles was performed by X-ray diffraction, Fourier transforms infrared spectroscopy (FTIR) and scanning electron microscopy with EDS. Prepared FeAl-LDH@SiO₂ particles were used as reinforcing agents in 1, 3 and 5 wt% quantity in poly (methyl) methacrylate matrix. The aim of this study was to examine whether FeAl-LDH@SiO₂ particles affect the mechanical properties of polymer composite materials. The morphology of the composites was examined using a field emission scanning electron microscope. Microindentation, tensile and impact testing determined the mechanical properties of the obtained composites.

SUBMITTER: Vuksanovic MM

PROVIDER: S-EPMC8479365 | biostudies-literature | 2021 Sep

REPOSITORIES: biostudies-literature

ACCESS DATA

Publications

Inorganically modified particles FeAl-LDH@SiO2 as reinforcement in poly (methyl) methacrylate matrix composite.

Vuksanović Marija M MM Egelja Adela A Barudžija Tanja T Tomić Nataša N Petrović Miloš M Marinković Aleksandar A Radojević Vesna V Heinemann Radmila Jančić RJ

Royal Society open science 20210929 9

Silica particles were obtained from rice husk to which layered double hydroxide particles were deposited (weight ratio 1 : 1). Fe2+-Al3+ layered double hydroxides (FeAl-LDH) were synthesized by co-precipitation with ratios Fe : Al of 3 : 1 in the presence of SiO2 particles from the rice husk. Characterization of the synthesized FeAl-LDH@SiO2 particles was performed by X-ray diffraction, Fourier transforms infrared spectroscopy (FTIR) and scanning elect ...[more]

PMID: 34631123

Similar Datasets

Project description:Fe-Al alloys in the aluminium range of 55-65 at.% exhibit a lamellar microstructure of B2-ordered FeAl and triclinic FeAl2, which is caused by a eutectoid decomposition of the high-temperature Fe5Al8 phase, the so-called ∊ phase. The orientation relationship of FeAl and FeAl2 has previously been studied by Bastin et al. [J. Cryst. Growth (1978 ▸), 43, 745] and Hirata et al. [Philos. Mag. Lett. (2008 ▸), 88, 491]. Since both results are based on different crystallographic data regarding FeAl2, the data are re-evaluated with respect to a recent re-determination of the FeAl2 phase provided by Chumak et al. [Acta Cryst. (2010 ▸), C66, i87]. It is found that both orientation relationships match subsequent to a rotation operation of 180° about a 〈112〉 crystallographic axis of FeAl or by applying the inversion symmetry of the FeAl2 crystal structure as suggested by the Chumak data set. Experimental evidence for the validity of the previously determined orientation relationships was found in as-cast fully lamellar material (random texture) as well as directionally solidified material (∼〈110〉FeAl || solidification direction) by means of orientation imaging microscopy and global texture measurements. In addition, a preferential interface between FeAl and FeAl2 was identified by means of trace analyses using cross sectioning with a focused ion beam. On the basis of these habit planes the orientation relationship between the two phases can be described by ([Formula: see text]01)FeAl || (114)[Formula: see text] and [111]FeAl || [1[Formula: see text]0][Formula: see text]. There is no evidence for twinning within FeAl lamellae or alternating orientations of FeAl lamellae. Based on the determined orientation and interface data, an atomistic model of the structure relationship of Fe5Al8, FeAl and FeAl2 in the vicinity of the eutectoid decomposition is derived. This model is analysed with respect to the strain which has to be accommodated at the interface of FeAl and FeAl2.

Dataset Information

Inorganically modified particles FeAl-LDH@SiO₂ as reinforcement in poly (methyl) methacrylate matrix composite.

Publications

Inorganically modified particles FeAl-LDH@SiO<sub>2</sub> as reinforcement in poly (methyl) methacrylate matrix composite.

Similar Datasets

OmicsDI is part of the ELIXIR infrastructure

Tweets