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N'-(4-Methoxy-benzyl-idene)-4-nitro-benzo-hydrazide methanol solvate.


ABSTRACT: The title compound, C(15)H(13)N(3)O(4)·CH(4)O, was synthesized from the reaction of 4-methoxy-benzaldehyde with 4-nitro-benzohydrazide in methanol. The benzene rings of the Schiff base mol-ecule are nearly coplanar, making a dihedral angle of 7.0?(3)°. The methanol solvent mol-ecules are linked to the Schiff base mol-ecules by N-H?O, O-H?N and O-H?O hydrogen bonds, forming chains running parallel to the b axis.

SUBMITTER: Wang YZ 

PROVIDER: S-EPMC2960903 | biostudies-other | 2008 Mar

REPOSITORIES: biostudies-other

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N'-(4-Methoxy-benzyl-idene)-4-nitro-benzo-hydrazide methanol solvate.

Wang Yuan-Zhi YZ   Wang Ming-Dong MD   Diao Yun-Peng YP   Cai Qian Q  

Acta crystallographica. Section E, Structure reports online 20080305 Pt 4


The title compound, C(15)H(13)N(3)O(4)·CH(4)O, was synthesized from the reaction of 4-methoxy-benzaldehyde with 4-nitro-benzohydrazide in methanol. The benzene rings of the Schiff base mol-ecule are nearly coplanar, making a dihedral angle of 7.0 (3)°. The methanol solvent mol-ecules are linked to the Schiff base mol-ecules by N-H⋯O, O-H⋯N and O-H⋯O hydrogen bonds, forming chains running parallel to the b axis. ...[more]

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