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3-Methoxy-benzaldehyde thio-semi-carbazone.

ABSTRACT: The title compound, C(9)H(11)N(3)OS, was prepared by the reaction of 3-methoxy-benzaldehyde and thio-semicarbazide. The benzyl-idene ring and the thio-semicarbazone fragment are slightly twisted, making a dihedral angle of 14.1?(1)°. A weak intra-molecular N-H?N hydrogen bond may influence the conformation of the mol-ecule. Inter-molecular N-H?S hydrogen bonds build up a three-dimensional network.

SUBMITTER: Zhang J

PROVIDER: S-EPMC2968893 | biostudies-other | 2009

REPOSITORIES: biostudies-other

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3-Methoxy-benzaldehyde thio-semi-carbazone.

Zhang Jian J Wu Lin-Ping LP Zhuang Ling-Hua LH Wang Guo-Wei GW

Acta crystallographica. Section E, Structure reports online 20090328 Pt 4

The title compound, C(9)H(11)N(3)OS, was prepared by the reaction of 3-methoxy-benzaldehyde and thio-semicarbazide. The benzyl-idene ring and the thio-semicarbazone fragment are slightly twisted, making a dihedral angle of 14.1 (1)°. A weak intra-molecular N-H⋯N hydrogen bond may influence the conformation of the mol-ecule. Inter-molecular N-H⋯S hydrogen bonds build up a three-dimensional network. ...[more]

PMID: 21582593

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