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N'-(5-Bromo-2-methoxy-benzyl-idene)-4-hydroxy-benzohydrazide methanol solvate.


ABSTRACT: In the title hydrazone compound, C(15)H(13)BrN(2)O(3)·CH(3)OH, the methanol solvate is linked to the benzohydrazide molecule through O-H?N and O-H?O hydrogen bonds. The benzohydrazide mol-ecule adopts an E configuration about the C=N double bond. The mol-ecule is twisted, with a dihedral angle between the two substituted benzene rings of 35.7?(2)°. In the crystal structure, mol-ecules are linked through inter-molecular N-H?O and O-H?O hydrogen bonds, forming layers parallel to the ac plane.

SUBMITTER: Lin XS 

PROVIDER: S-EPMC2969367 | biostudies-other | 2009 Jun

REPOSITORIES: biostudies-other

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N'-(5-Bromo-2-methoxy-benzyl-idene)-4-hydroxy-benzohydrazide methanol solvate.

Lin Xue-Song XS   Sang Ya-Li YL  

Acta crystallographica. Section E, Structure reports online 20090620 Pt 7


In the title hydrazone compound, C(15)H(13)BrN(2)O(3)·CH(3)OH, the methanol solvate is linked to the benzohydrazide molecule through O-H⋯N and O-H⋯O hydrogen bonds. The benzohydrazide mol-ecule adopts an E configuration about the C=N double bond. The mol-ecule is twisted, with a dihedral angle between the two substituted benzene rings of 35.7 (2)°. In the crystal structure, mol-ecules are linked through inter-molecular N-H⋯O and O-H⋯O hydrogen bonds, forming layers parallel to the ac plane. ...[more]

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