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(E)-2-(Isonicotinoylhydrazonometh-yl)benzoic acid methanol monosolvate.

ABSTRACT: The title compound, C(14)H(11)N(3)O(3)·CH(4)O, was synthesized by the condensation reaction of isonicotinohydrazide with an equimolar quantity of 2-formyl-benzoic acid in methanol. The hydrazone mol-ecule displays an E configuration about the C=N bond. The dihedral angel between the pyridine and the benzene rings is 12.04?(5)°. In the crystal structure, mol-ecules are linked by O-H?N, O-H?O and N-H?O hydrogen-bonding inter-actions.

SUBMITTER: Li W 

PROVIDER: S-EPMC2970267 | biostudies-other | 2009

REPOSITORIES: biostudies-other

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(E)-2-(Isonicotinoylhydrazonometh-yl)benzoic acid methanol monosolvate.

Li Wenkuan W   Yin Handong H   Wen Liyuan L   Cui Jichun J   Wang Daqi D  

Acta crystallographica. Section E, Structure reports online 20090930 Pt 10

The title compound, C(14)H(11)N(3)O(3)·CH(4)O, was synthesized by the condensation reaction of isonicotinohydrazide with an equimolar quantity of 2-formyl-benzoic acid in methanol. The hydrazone mol-ecule displays an E configuration about the C=N bond. The dihedral angel between the pyridine and the benzene rings is 12.04 (5)°. In the crystal structure, mol-ecules are linked by O-H⋯N, O-H⋯O and N-H⋯O hydrogen-bonding inter-actions. ...[more]

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