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N'-(3-Methoxy-benzyl-idene)-4-nitro-benzohydrazide monohydrate.

ABSTRACT: There are two independent formula units in the asymmetric unit of the title compound, C(15)H(13)N(3)O(4)·H(2)O. The C=C-N-C torsion angle of the methyl-idenehydrazide group is 174.3?(2)° in one mol-ecule and 178.6?(2)° in the other. The dihedral angles between the two benzene rings in the two mol-ecules are 4.17?(12) and 3.58?(12)°. In the crystal structure, inter-molecular O-H?O, N-H?O and O-H?N hydrogen bonds link the components into a two-dimensional network and additional stabilization is provided by weak inter-molecular C-H?O hydrogen bonds.

SUBMITTER: Ahmad T 

PROVIDER: S-EPMC2983820 | biostudies-other | 2010 Mar

REPOSITORIES: biostudies-other

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N'-(3-Methoxy-benzyl-idene)-4-nitro-benzohydrazide monohydrate.

Ahmad Tanveer T   Zia-Ur-Rehman Muhammad M   Siddiqui Hamid Latif HL   Fasih Ullah Muhammad M   Parvez Masood M  

Acta crystallographica. Section E, Structure reports online 20100331 Pt 4

There are two independent formula units in the asymmetric unit of the title compound, C(15)H(13)N(3)O(4)·H(2)O. The C=C-N-C torsion angle of the methyl-idenehydrazide group is 174.3 (2)° in one mol-ecule and 178.6 (2)° in the other. The dihedral angles between the two benzene rings in the two mol-ecules are 4.17 (12) and 3.58 (12)°. In the crystal structure, inter-molecular O-H⋯O, N-H⋯O and O-H⋯N hydrogen bonds link the components into a two-dimensional network and additional stabilization is pr  ...[more]

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