Unknown

Dataset Information

0

6-Methyl-2,3,4,9-tetra-hydro-1H-carbazole-1-thione.

ABSTRACT: In the title mol-ecule, C(13)H(13)NS, the dihedral angle between the benzene ring and the fused pyrrole ring is 0.71?(8)° and the cyclo-hexene ring is in an envelope form. The (CH(2))(3) atoms of the cyclo-hexene ring are disordered over two positions; the site-occupancy factor for the major component refined to 0.862?(4). In the crystal, inter-molecular N-H?S hydrogen bonds lead to the formation of centrosymmetric aggregates via an R(2) (2)(10) ring.

SUBMITTER: Archana R 

PROVIDER: S-EPMC3151814 | biostudies-other | 2011 Jul

REPOSITORIES: biostudies-other

Json Xml
altmetric image

Publications

6-Methyl-2,3,4,9-tetra-hydro-1H-carbazole-1-thione.

Archana R R   Prabakaran K K   Rajendra Prasad K J KJ   Thiruvalluvar A A   Butcher R J RJ  

Acta crystallographica. Section E, Structure reports online 20110611 Pt 7

In the title mol-ecule, C(13)H(13)NS, the dihedral angle between the benzene ring and the fused pyrrole ring is 0.71 (8)° and the cyclo-hexene ring is in an envelope form. The (CH(2))(3) atoms of the cyclo-hexene ring are disordered over two positions; the site-occupancy factor for the major component refined to 0.862 (4). In the crystal, inter-molecular N-H⋯S hydrogen bonds lead to the formation of centrosymmetric aggregates via an R(2) (2)(10) ring. ...[more]

Similar Datasets

Unknown 4a-Methyl-2,3,4,4a-tetra-hydro-1H-carbazole-6-sulfonamide.
| S-EPMC3344011 | biostudies-literature
Unknown 2,3,4,9-Tetra-hydro-1H-carbazole.
| S-EPMC2960078 | biostudies-literature
Unknown (±)-4a-(4-Nitro-benz-yl)-2,3,4,4a-tetra-hydro-1H-carbazole.
| S-EPMC3152074 | biostudies-literature
Unknown Ethyl 4-oxo-2,3,4,9-tetra-hydro-1H-carbazole-3-carboxyl-ate.
| S-EPMC3120486 | biostudies-literature
Unknown 8-Methyl-2,3,4,9-tetra-hydro-1H-carbazol-1-one.
| S-EPMC3007954 | biostudies-literature
Unknown 3,3,6,6-Tetra-methyl-9-[6-(3,3,6,6-tetra-methyl-1,8-dioxo-2,3,4,5,6,7,8,9-octa-hydro-1H-xanthen-9-yl)pyridin-2-yl]-2,3,4,5,6,7,8,9-octa-hydro-1H-xanthene-1,8-dione.
| S-EPMC3100053 | biostudies-literature
Unknown 4-Methyl-2-oxo-2,3,4,5-tetra-hydro-1H-1,5-benzodiazepine-5-carbaldehyde.
| S-EPMC2970231 | biostudies-literature
Unknown 6-Methyl-pyridine-2(1H)-thione.
| S-EPMC2979122 | biostudies-literature
Unknown 5-Chloro-acetyl-4-methyl-2,3,4,5-tetra-hydro-1H-1,5-benzodiazepin-2-one.
| S-EPMC2970477 | biostudies-literature
Unknown 2-(6-Methyl-2,3,4,9-tetra-hydro-1H-carbazol-1-yl-idene)propane-dinitrile.
| S-EPMC3238928 | biostudies-literature