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1,3-Benzothia-zole-oxalic acid (2/1).

ABSTRACT: The asymmetric unit of the title compound, C(7)H(5)NS·0.5C(2)H(2)O(4), contains one benzothia-zole mol-ecule and half an oxalic acid mol-ecule, the complete mol-ecule being generated by inversion symmetry. The benzothia-zole mol-ecule is essentially planar, with a maximum deviation of 0.007?(1)?Å. In the crystal, the benzothia-zole mol-ecules inter-act with the oxalic acid mol-ecules via O-H?N and C-H?O hydrogen bonds generating R(2) (2)(8) (× 2) and R(4) (4)(10) motifs, thereby forming supra-molecular ribbons along [101].

SUBMITTER: Abdalsalam AA

PROVIDER: S-EPMC3200845 | biostudies-other | 2011 Sep

REPOSITORIES: biostudies-other

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1,3-Benzothia-zole-oxalic acid (2/1).

Abdalsalam Ashraf Ahmad Ali AA Al-Dajani Mohammad T M MT Mohamed Nornisah N Hemamalini Madhukar M Fun Hoong-Kun HK

Acta crystallographica. Section E, Structure reports online 20110817 Pt 9

The asymmetric unit of the title compound, C(7)H(5)NS·0.5C(2)H(2)O(4), contains one benzothia-zole mol-ecule and half an oxalic acid mol-ecule, the complete mol-ecule being generated by inversion symmetry. The benzothia-zole mol-ecule is essentially planar, with a maximum deviation of 0.007 (1) Å. In the crystal, the benzothia-zole mol-ecules inter-act with the oxalic acid mol-ecules via O-H⋯N and C-H⋯O hydrogen bonds generating R(2) (2)(8) (× 2) and R(4) (4)(10) motifs, thereby forming supra-mo ...[more]

PMID: 22065811

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