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1,2-Bis(2,4-di-nitro-phen-yl)disulfane.

ABSTRACT: In the title mol-ecule, C12H6N4O8S2, the dihedral angle between the benzene rings is 77.00?(8)°. The mean planes of the nitro groups are twisted slightly from the benzene rings, forming dihedral angles in the range 2.3?(2)-8.6?(3)°. The S-S bond length is 2.0458?(7)?Å. Each S atom is essentially coplanar with the benzene ring to which it is attached, with deviations from the ring planes of 0.0163?(5) and 0.0538?(5)?Å. In the crystal, mol-ecules are linked through weak C-H?O hydrogen bonds, forming a two-dimensional network parallel to (001).

SUBMITTER: Muthulakshmi S

PROVIDER: S-EPMC3648327 | biostudies-other | 2013 May

REPOSITORIES: biostudies-other

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1,2-Bis(2,4-di-nitro-phen-yl)disulfane.

Muthulakshmi Selvarasu S Kalaivani Doraisamyraja D

Acta crystallographica. Section E, Structure reports online 20130430 Pt 5

In the title mol-ecule, C12H6N4O8S2, the dihedral angle between the benzene rings is 77.00 (8)°. The mean planes of the nitro groups are twisted slightly from the benzene rings, forming dihedral angles in the range 2.3 (2)-8.6 (3)°. The S-S bond length is 2.0458 (7) Å. Each S atom is essentially coplanar with the benzene ring to which it is attached, with deviations from the ring planes of 0.0163 (5) and 0.0538 (5) Å. In the crystal, mol-ecules are linked through weak C-H⋯O hydrogen bonds, formi ...[more]

PMID: 23723947

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