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A general synthetic route to [Cu(X)(NHC)] (NHC = N-heterocyclic carbene, X = Cl, Br, I) complexes.

ABSTRACT: A one-pot procedure for the synthesis of [Cu(X)(NHC)] (X = Cl, Br, I) is reported. The reaction is applicable to a wide range of saturated and unsaturated NHC ligands, is scalable and proceeds under mild conditions using technical grade solvents in air.

SUBMITTER: Santoro O 

PROVIDER: S-EPMC4155829 | biostudies-other | 2013 Nov

REPOSITORIES: biostudies-other

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A general synthetic route to [Cu(X)(NHC)] (NHC = N-heterocyclic carbene, X = Cl, Br, I) complexes.

Santoro Orlando O   Collado Alba A   Slawin Alexandra M Z AM   Nolan Steven P SP   Cazin Catherine S J CS  

Chemical communications (Cambridge, England) 20131101 89

A one-pot procedure for the synthesis of [Cu(X)(NHC)] (X = Cl, Br, I) is reported. The reaction is applicable to a wide range of saturated and unsaturated NHC ligands, is scalable and proceeds under mild conditions using technical grade solvents in air. ...[more]

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